Abstract
[HOs3(CO)10{CF3C:C(H)CF3}] reacts with carbon monoxide to give the complexes cis- and trans-[Os3(CO)11–{CF3(H)C:C(H)CF3}], which react further with CO to liberate free alkenes and generate [Os3(CO)12]; an X-ray diffraction study of the cis-isomer is the first for a mono-substituted alkene derivative of a binary metal carbonyl cluster.
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