Abstract

AbstractThe cold stage specimen surface in our Balzer's 300 Freeze‐etch instrument, averages 29–43°C warmer than the reading on the GA‐1 stage temperature control unit. By introduction of Indium foil seals above and below the stainless steel plug in the stage tower, the specimen cold stage surface temperatures were still 9–10°C warmer than the GA‐1 reading. After replacing the stainless steel plug with a copper plug and using Indium seals, the cold stage specimen surface was brought within 2.6°C of the GA‐1 temperature reading. In addition, the copper plug, Indium seal modified stage cools about two times faster in going from –100°C to –150°C than the normal stainless steel stage modified with Indium seals.

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