Abstract

The four-ring system in the title compound, C16H9NO2·CH3OH, is planar (r.m.s deviation = 0.03 Å); the methanol solvent mol­ecule forms a hydrogen bond to the quinoline N atom.

Highlights

  • The four-ring system in the title compound, C16H9NO2ÁCH3OH, is planar (r.m.s deviation = 0.03 A ); the methanol solvent molecule forms a hydrogen bond to the quinoline N atom

  • Related literature The compound in this study was synthesized from the cyclization of 2-(quinolin-8-yloxy)benzoic acid; for the synthesis of this acid, see: Chen et al (2007)

  • Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: XU2605)

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Summary

Structure Reports Online

Key indicators: single-crystal X-ray study; T = 295 K; mean (C–C) = 0.003 A; R factor = 0.046; wR factor = 0.147; data-to-parameter ratio = 13.8. The four-ring system in the title compound, C16H9NO2ÁCH3OH, is planar (r.m.s deviation = 0.03 A ); the methanol solvent molecule forms a hydrogen bond to the quinoline N atom. Related literature The compound in this study was synthesized from the cyclization of 2-(quinolin-8-yloxy)benzoic acid; for the synthesis of this acid, see: Chen et al (2007). For the synthesis by the Skraup reaction of amino-9H-xanthene-9-one, see: Fujiwara & Okabayashi (1994)

Data collection
HÁ Á ÁA
Bruker APEXII diffractometer
Full Text
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