Abstract
The title compound, C11H11N3, was synthesized as part of our research into functionalized pyrimidines. It crystallizes with two independent molecules in the asymmetric unit that differ only in the twist between the two aromatic rings; the torsion angles between the rings are 29.9 (2) and 45.1 (2)°. The crystal packing is dominated by intermolecular N—H⋯N hydrogen bonds between independent and equivalent molecules, forming an infinite three-dimensional network.
Highlights
The title compound, C11H11N3, was synthesized as part of our research into functionalized pyrimidines. It crystallizes with two independent molecules in the asymmetric unit that differ only in the twist between the two aromatic rings; the torsion angles between the rings are 29.9 (2) and 45.1 (2)
The crystal packing is dominated by intermolecular N—HÁ Á ÁN hydrogen bonds between independent and equivalent molecules, forming an infinite three-dimensional network
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: FL2182)
Summary
Absorption correction: multi-scan (SADABS; Sheldrick, 2004) Tmin = 0.977, Tmax = 0.985. Z=8 Mo K radiation = 0.08 mmÀ1 T = 273 (2) K 0.30 Â 0.20 Â 0.20 mm 17472 measured reflections 3619 independent reflections 2760 reflections with I > 2(I) Rint = 0.033. The title compound, C11H11N3, was synthesized as part of our research into functionalized pyrimidines. It crystallizes with two independent molecules in the asymmetric unit that differ only in the twist between the two aromatic rings; the torsion angles between the rings are 29.9 (2) and 45.1 (2). The crystal packing is dominated by intermolecular N—HÁ Á ÁN hydrogen bonds between independent and equivalent molecules, forming an infinite three-dimensional network
Sign-in/Register to view highlights & summary Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callMore From: Acta Crystallographica Section E Structure Reports Online
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
