Abstract
In the title compound, C13H9Cl2NO3S·H2O, the conformation of the C=O bond is syn to the meta-Cl group in the benzoyl ring. The molecules are twisted at the S—N bond with a C—S—N—C torsion angle of 72.9 (2)°. The dihedral angle between the sulfonyl benzene ring and the S—NH—C—O segment is 77.8 (1)° and that between the sulfonyl and benzoyl benzene rings is 80.5 (1)°. In the crystal, molecules are linked into a two-dimensional network parallel to (100) by N—H⋯O and O—H⋯O hydrogen bonds.
Highlights
In the title compound, C13H9Cl2NO3SH2O, the conformation of the C O bond is syn to the meta-Cl group in the benzoyl ring
The molecules are twisted at the S—N bond with a C—
Molecules are linked into a two-dimensional network parallel to (100) by N—
Summary
Thimme Gowda,a* Sabine Forob and Hartmut Fuessb a Department of Chemistry, Mangalore University, Mangalagangotri 574 199, Mangalore, India, and bInstitute of Materials Science, Darmstadt University of Technology, Petersenstrasse 23, D-64287 Darmstadt, Germany. C13H9Cl2NO3SH2O, the conformation of the C O bond is syn to the meta-Cl group in the benzoyl ring. The molecules are twisted at the S—N bond with a C—. The dihedral angle between the sulfonyl benzene ring and the S—NH—C—O segment is 77.8 (1) and that between the sulfonyl and benzoyl benzene rings is 80.5 (1). Data collection: CrysAlis CCD (Oxford Diffraction, 2009); cell refinement: CrysAlis RED (Oxford Diffraction, 2009); data reduction: CrysAlis RED; program(s) used to solve structure: SHELXS97. (Sheldrick, 2008); molecular graphics: PLATON (Spek, 2009); software used to prepare material for publication: SHELXL97
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