Abstract
AbstractHomologous 4,5‐dihydro‐5‐thioxo‐1H‐tetrazole‐l‐alkanoic and alkanesulfonic acids were prepared by reaction of sodium azide with methyl (carboxyalkyl)‐ and (sulfoalkyl) carbamodithioates, respectively. 4,5‐Dihydro‐5‐thioxo‐1H‐tetrazole‐i‐alkanamides were derived from the corresponding alkanoic acids by aminolysis of their acid chlorides or imidazolides. Analogous alkane‐sulfonamides were synthesized by the reaction of methyl [[[(1,1‐dimethylethyl) amino]sulfonyl]‐alkyljcarbamodithioates with sodium azide followed by removal of the 1,1‐dimethylethyl group with trifluoroacetic acid.
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