Abstract

The title compound, crystallized as a methanol solvate, C18H20O2·CH3OH, is an inter­mediate in the synthesis of the anti­lipidemic agent clinofibrate. Mol­ecules are packed together with the methanol solvent molecule via two O—H⋯O hydrogen bonds. The third O—H⋯O hydrogen bond is between neighboring 4,4′-(cyclo­hexane-1,1-di­yl)diphenol mol­ecules. The dihedral angle between two benzene rings planes is 81.69 (6).

Highlights

  • The title compound, crystallized as a methanol solvate, C18H20O2CH3OH, is an intermediate in the synthesis of the antilipidemic agent clinofibrate

  • We present the crystal structure of the title compound(I)

  • The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry

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Summary

Refinement a

R factor = 0.058; wR factor = 0.182; data-to-parameter ratio = 14.5. The title compound, crystallized as a methanol solvate, C18H20O2CH3OH, is an intermediate in the synthesis of the antilipidemic agent clinofibrate. Molecules are packed together with the methanol solvent molecule via two O—. The third O—H O hydrogen bond is between neighboring 4,40 -(cyclohexane-1,1-diyl)diphenol molecules. The dihedral angle between two benzene rings planes is 81.69 (6)

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