Abstract
The asymmetric unit of the title compound, C14H14ClNO2S, contains two independent molecules. The torsion angles of the C—SO2—NH—C segments in the two molecules are −76.5 (5) and −48.3 (4)°. The two aromatic rings are tilted relative to each other by 76.6 (2)° in one molecule and 70.7 (2)° in the other. In the crystal structure, intermolecular N—H⋯O hydrogen bonds link the molecules into centrosymmetric dimers.
Highlights
Structure ReportsG. Nirmalaa and Hartmut Fuessb a Department of Chemistry, Mangalore University, Mangalagangotri 574 199, Mangalore, India, and bInstitute of Materials Science, Darmstadt University of Technology, Petersenstrasse 23, D-64287 Darmstadt, Germany
The asymmetric unit of the title compound, C14H14ClNO2S, contains two independent molecules
The prism like colourless single crystals used in X-ray diffraction studies were grown in ethanolic solution by slow evaporation at room temperature
Summary
G. Nirmalaa and Hartmut Fuessb a Department of Chemistry, Mangalore University, Mangalagangotri 574 199, Mangalore, India, and bInstitute of Materials Science, Darmstadt University of Technology, Petersenstrasse 23, D-64287 Darmstadt, Germany. Symmetry code: (i) x þ 1; y þ 1; z þ 1. R factor = 0.097; wR factor = 0.317; data-to-parameter ratio = 13.9. The asymmetric unit of the title compound, C14H14ClNO2S, contains two independent molecules. The two aromatic rings are tilted relative to each other by 76.6 (2) in one molecule and. N—H O hydrogen bonds link the molecules into centrosymmetric dimers
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