Abstract
A new 3D organic-inorganic hybrid complex, H2K2[HN(CH2CH2OH)3]2[Cu2(C2H6O2)4Cl][Mo8O26]·17H2O (1) has been synthesized and structurally characterized. In compound 1, the [β-Mo8O26]4− units and 1D {Cu2(C2H6O2)4Cl}n chains are joined together via K+ ions, leading to the 3D porous framework. The magnetic measurements of 1 indicates the presence of antiferromagnetic interactions between copper(II) ions. Electrochemical experiments reveal that 1-CPE exhibits the characteristic multi-electron redox processes ascribed to MoVI centers, and shows good electrocatalytic activity for H2O2 reduction.
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