Abstract
In the title compound, C16H15ClN2O3·H2O, the water molecule is linked to the Schiff base molecule via an O—H⋯O hydrogen bond. In the Schiff base molecule, an intramolecular O—H⋯N hydrogen bond occurs and the dihedral angle between the two benzene rings is 20.5 (5)°. In the crystal, the Schiff base and water molecules are linked by intermolecular N—H⋯O and O—H⋯O hydrogen bonds, forming layers in the ab plane.
Highlights
C16H15ClN2O3H2O, the water molecule is linked to the Schiff base molecule via an O—H O
The title compound was prepared by the method described in Zhu (2010)
In the last few years, a number of Schiff bases derived from the reaction of aldehydes with benzohydrazides were prepared and structurally characterized (Bessy et al, 2006; Podyachev et al, 2007; Raj & Kurup, 2007; Pouralimardan et al, 2007; Bacchi et al, 2006; Dinda et al, 2002)
Summary
R factor = 0.067; wR factor = 0.158; data-to-parameter ratio = 15.8. H atoms treated by a mixture of independent and constrained refinement max = 0.20 e Å3. C16H15ClN2O3H2O, the water molecule is linked to the Schiff base molecule via an O—H O hydrogen bond. In the Schiff base molecule, an intramolecular. O—H N hydrogen bond occurs and the dihedral angle between the two benzene rings is 20.5 (5). The Schiff base and water molecules are linked by intermolecular. N—H O and O—H O hydrogen bonds, forming layers in the ab plane
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