Abstract
Abstract A solid-state NMR method combining 27Al multiple-quantum magic-angle spinning (MQMAS) and 31P{27Al} heteronuclear correlation (HETCOR) has been applied for the structural analysis of amorphous AlPO4. We obtained a correlation between the isotropic chemical shifts of 31P in PO4 and of 27Al in each AlOn (n = 4, 5, and 6) distributed by the amorphous structure.
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