Abstract
Methyl 3,6-thioanhydro-α-D-glucopyranoside ( 5) was obtained in seven steps from the commercially available methyl α-D-glucopyranoside. Transformation of 5 into (2 R,3 R,4 S)-3,4-dihydroxy-2-[( S)-1,2-dihydroxyethyl]thiolane ( 9) was achieved by acid hydrolysis and subsequent reduction without isolation of its formyl derivative ( 8).
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