Abstract

In the title thio­urea derivative, C10H17N3O2S, the carboxyl group and the least-squares plane through the cyclo­hexyl ring are twisted out of the plane through the central CN3S residue; the respective dihedral angles are 7.18 (8) and 62.29 (4)°. The conformation about the azomethine bond [1.275 (2) Å] is E. The NH groups are anti, with one forming an intra­molecular N—H⋯N hydrogen bond. The main feature of the crystal structure is the formation of linear supra­molecular chains along [110] mediated by alternating pairs of O—H⋯O and pairs of N—H⋯S hydrogen bonds.

Highlights

  • In the title thiourea derivative, C10H17N3O2S, the carboxyl group and the least-squares plane through the cyclohexyl ring are twisted out of the plane through the central CN3S residue; the respective dihedral angles are 7.18 (8) and 62.29 (4)

  • The main feature of the crystal structure is the formation of linear supramolecular chains along [110] mediated by alternating pairs of O—H O and pairs of N—H S hydrogen bonds

  • Universiti Malaysia Sarawak (UNIMAS) for the facilities to carry out the research work

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Summary

Agilent Supernova Dual diffractometer with an Atlas detector

The main feature of the crystal structure is the formation of linear supramolecular chains along [110] mediated by alternating pairs of O—H O and pairs of N—H S hydrogen bonds

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Mo K radiation
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