Abstract
In the crystal structure of the title compound, C16H14F3N3OS·C3H8O, the molecules are linked into chains along [010] via N—H⋯O and O—H⋯N hydrogen bonds. The triclinic form was reported by Ren et al. [(2011). Acta Cryst. E67, o270] and the first monoclinic form by Chen et al. [(2012). Acta Cryst. E68, o2015–o2016]. The fused five-and six-membered rings make a dihedral angle of 1.22 (2)°, while the benzene and pyridine rings make a dihedral angle of 10.15 (2)°.
Highlights
Bruker APEXII diffractometerRefinement a School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou
In the crystal structure of the title compound, C16H14F3N3OSC3H8O, the molecules are linked into chains along [010] via
The triclinic form was reported by Ren et al [(2011)
Summary
Refinement a School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou. 450001, People’s Republic of China, bPharmaceutical Crystal Engineering Research. Shanghai Institute of Pharmaceutical Industry, 1320 Beijing Road (West), Shanghai 200040, People’s Republic of China, and cNational Engineering Laboratory for Cereal Fermentation Technology, School of Chemical & Material Engineering, Jiangnan University, Wuxi 214122, People’s Republic of China. R factor = 0.040; wR factor = 0.116; data-to-parameter ratio = 13.4. Symmetry codes: (i) x; y; z 1; (ii) x; y 1; z þ 1. In the crystal structure of the title compound, C16H14F3N3OSC3H8O, the molecules are linked into chains along [010] via. The triclinic form was reported by Ren et al [(2011). E67, o270] and the first monoclinic form by Chen et al [(2012). The fused five-and six-membered rings make a dihedral angle of 1.22 (2) , while the benzene and pyridine rings make a dihedral angle of 10.15 (2)
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