Abstract

The asymmetric unit of the title hydrated salt, C24H35N2O5 +·Cl−·2H2O, contains one organic cation that has its protonation site at the amine function, one chloride anion and two lattice water mol­ecules. In the crystal, one pair of lattice water mol­ecules and two chloride anions form a four-membered centrosymmetric hydrogen-bond cycle. In addition, O—H⋯O, N—H⋯O and N—H⋯Cl hydrogen bonds involving the N—H groups, the water mol­ecules and the C=O group are observed. As a result, a hydrogen-bonded layer parallel to (100) is formed. The thickness of such a layer corresponds to the length of the a axis [21.977 (3) Å].

Highlights

  • H atoms treated by a mixture of independent and constrained refinement max = 0.20 e Å3

  • A hydrogen-bonded layer parallel to (100) is formed. The thickness of such a layer corresponds to the length of the a axis [21.977 (3) Å]

  • Supporting information for this paper is available from the IUCr electronic archives (Reference: WM2799)

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Summary

Structure Reports

Data collection [2-(3,4-Dimethoxyphenyl)ethyl](3-{N-[2(3,4-dimethoxyphenyl)ethyl]carbamoyl}propyl)azanium chloride dihydrate S. Yunusov Institute of the Chemistry of Plant Substances, Academy of Sciences of Uzbekistan, Mirzo Ulugbek Str. 77, Tashkent 100170, Uzbekistan

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Graphite monochromator
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