Abstract
The title racemate, C7H10O3, aggregates in the solid as acid-to-ketone hydrogen-bonding catemers [O⋯O = 2.7050 (13) Å and O—H⋯O = 166.1 (17)°] having glide-related components. Four such heterochiral chains, paired centrosymmetrically about (, , ) in the cell, proceed through the cell in the 010 direction, with alignment with respect to the c axis of ++−−.
Highlights
The title racemate, C7H10O3, aggregates in the solid as acid-toketone hydrogen-bonding catemers [O O = 2.7050 (13) Å and O—H O = 166.1 (17) ] having glide-related components
010 direction, with alignment with respect to the c axis of HWT is grateful to Professor Gree Loober Spoog for helpful consultations
EG and HWT express their gratitude to Sanofi–Aventis for a grant in support of undergraduate research in organic synthesis
Summary
Olson Memorial Laboratories, Department of Chemistry, Rutgers University, Newark, NJ 07102, USA. The title racemate, C7H10O3, aggregates in the solid as acid-toketone hydrogen-bonding catemers [O O = 2.7050 (13) Å and O—H O = 166.1 (17) ] having glide-related components. Four such heterochiral chains, paired centrosymmetrically about (12, 12, 12) in the cell, proceed through the cell in the. EG and HWT express their gratitude to Sanofi–Aventis for a grant in support of undergraduate research in organic synthesis. This paper is dedicated to the memory of HWT; he was a dedicated mentor, teacher and friend at Rutgers University-Newark for over 40 years
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