Abstract
In the title compound, C14H13ClN4S, obtained from a reaction of 2-benzoyl-4-chloroaniline with thiosemicarbazide in ethanol, the dihedral angle between the aromatic rings is 81.31 (13)°. In the crystal, the molecules are linked by three N—H⋯S hydrogen bonds, forming centrosymmetric rings with set-graph motif R 2 2(8) and R 2 2(18), and resulting in the formation of a two-dimensional network lying parallel to (010).
Highlights
In the title compound, C14H13ClN4S, obtained from a reaction of 2-benzoyl-4-chloroaniline with thiosemicarbazide in ethanol, the dihedral angle between the aromatic rings is
H atoms treated by a mixture of independent and constrained refinement max = 0.54 e Å3
Supporting information for this paper is available from the IUCr electronic archives (Reference: BX2459)
Summary
Escola de Quımica e Alimentos, Universidade Federal do Rio Grande, Av. Itália km. 08, Campus Carreiros, 96203-900, Rio Grande-RS, Brazil, bDepartamento de Quımica, Universidade Federal de Santa Maria, Av. Roraima, Campus, 97105-900, Santa Maria-RS, Brazil, and cDepartamento de Quımica, Universidade Federal de Sergipe, Av. Marechal Rondon s/n, Campus, 49100-000, São Cristóvão-SE, Brazil
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