Abstract
The title compound, C11H9N5O2S, was synthesized from N-phthaloylglycine and thiocarbohydrazide by the fusion method. This is the first report of a triazole derivative of N-phthaloylglycine. The title compound exists in the thione form. The molecule is non-planar, with a dihedral angle between the isoindoline ring system and the triazole ring system of 82.24 (5)°. The crystal structure is stabilized by intermolecular hydrogen bonding linking the molecules into a three-dimensional network.
Highlights
The title compound, C11H9N5O2S, was synthesized from N-phthaloylglycine and thiocarbohydrazide by the fusion method. This is the first report of a triazole derivative of Nphthaloylglycine
The title compound exists in the thione form
The crystal structure is stabilized by intermolecular hydrogen bonding linking the molecules into a threedimensional network
Summary
Key indicators: single-crystal X-ray study; T = 100 K; mean (C–C) = 0.003 A; R factor = 0.029; wR factor = 0.070; data-to-parameter ratio = 12.8. The title compound, C11H9N5O2S, was synthesized from N-phthaloylglycine and thiocarbohydrazide by the fusion method. This is the first report of a triazole derivative of Nphthaloylglycine. The title compound exists in the thione form. The molecule is non-planar, with a dihedral angle between the isoindoline ring system and the triazole ring system of 82.24 (5). The crystal structure is stabilized by intermolecular hydrogen bonding linking the molecules into a threedimensional network
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