Abstract
In the cation of the title salt, C23H27N2O4 +·C2HO4 −·2H2O, both fused pyrrolidine rings exhibit twisted conformations, while the piperidine rings adopt screw-boat and boat conformations. In the crystal, the three components are linked via O—H⋯O and N—H⋯O interactions, forming a tape along the b axis. The tapes are further linked by weak C—H⋯O hydrogen bonds. forming a three-dimensional network.
Highlights
In the cation of the title salt, C23H27N2O4+C2HO42H2O, both fused pyrrolidine rings exhibit twisted conformations, while the piperidine rings adopt screw-boat and boat conformations
H atoms treated by a mixture of independent and constrained refinement max = 0.33 e Å3
The three components are linked via O—H O and N—H O interactions, forming a tape along the b axis
Summary
H atoms treated by a mixture of independent and constrained refinement max = 0.33 e Å3. Min = 0.32 e Å3 a Department of Physics, Presidency College, Chennai 600 005, India, and Department of Physics, CPCL Polytechnic College, Chennai 600 068, India. R factor = 0.042; wR factor = 0.116; data-to-parameter ratio = 16.4. In the cation of the title salt, C23H27N2O4+C2HO42H2O, both fused pyrrolidine rings exhibit twisted conformations, while the piperidine rings adopt screw-boat and boat conformations. The three components are linked via O—H O and N—H O interactions, forming a tape along the b axis. The tapes are further linked by weak C—.
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