Abstract

In the toluene hemisolvated tripodal tris­(2-amino­ethyl)amine Schiff base, C30H33Cl3N4O3·0.5C7H8, one of the three imino N atoms is protonated, forming a hydrogen bond with the O atom at an adjacent benzene ring. The other two imino N atoms act as hydrogen-bond acceptors from phenolate OH groups. The toluene solvent mol­ecule is disordered about a centre of inversion.

Highlights

  • Structure Reports OnlineKey indicators: single-crystal X-ray study; T = 100 K; mean (C–C) = 0.004 A; disorder in solvent or counterion; R factor = 0.050; wR factor = 0.150; data-toparameter ratio = 17.7

  • In the toluene hemisolvated tripodal tris(2-aminoethyl)amine Schiff base, C30H33Cl3N4O3Á0.5C7H8, one of the three imino N atoms is protonated, forming a hydrogen bond with the O atom at an adjacent benzene ring

  • The other two imino N atoms act as hydrogen-bond acceptors from phenolate OH groups

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Summary

Structure Reports Online

Key indicators: single-crystal X-ray study; T = 100 K; mean (C–C) = 0.004 A; disorder in solvent or counterion; R factor = 0.050; wR factor = 0.150; data-toparameter ratio = 17.7

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