Abstract
The mass spectra of per(trimethylsilyl) ethers of desulfated glucosinolates are dominated by ions derived from the glucose moiety. The ions at m/e 271 and 361 are much more abundant than in the spectra shown by the corresponding derivatives of hexoses and their simple glycosides. The individual glucosinolates are distinguished by a few ions originating from their respective aglycon groups. The 1H- and 13C-N.M.R. spectra of sinigrin and some closely related compounds have been analyzed.
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