Abstract

AbstractThe 17O NMR spectra of 17O isotope‐enriched tributyltin(IV) acetate (1) and dibutyltin(IV) diacetate (2) were recorded in various solvents over wide temperature ranges. Only a single 17O signal was observed for both oxygen atoms of the —COOSn—groups under these experimental conditions, in both non‐coordinating and coordinating solvents. The 17O NMR spectra of tert‐butyl acetate (3) were obtained for comparison. Copyright © 2002 John Wiley & Sons, Ltd.

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