Abstract
14N NMR of magnetically oriented microcrystals is reported. With a home-built 1H–13C–14N probe capable of modulating the rotation of the sample around the axis normal to the magnetic field, magnetically oriented microcrystal suspension (MOMS) of l-alanine is made. 14N NMR spectra acquired with various timings during intermittent rotation lead to a rotation pattern of the MOMS similar to that of a single crystal. The effect of orientational distribution of the microcrystals to broadening of the resonance line is discussed.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have