Abstract
Abstract: 2-methoxycarbonylethyldichlorotin hydroxide, CH 3 OCOCH 2 CH 2 SnCl 2 (OH) ( 1), has been synthesized by hydrolysis reaction and characterized by elemental analysis, FTIR, 1 H NMR spectroscopy, and X-ray single crystal diffraction. Compound 1 is a centrosymmetric dimmer, and the tin atom approximates to octahedral geometry via an intramolecular carbonyl- to-tin coordination and hydroxo-bridging. The compound display high selectivity and good catalysis activity on the transesterification reaction of ethyl acetoacetate with an alcohol. Supporting information: FT-IR, 1 H NMR, X-Ray, GC/MS analyses, Cif file.
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