Abstract
12-Tungstophosphoric heteropolyacid anions (denoted PW 12) have been successfully immobilised on chemically modified mesoporous silica FSM-16 (denoted FSM-16 (m)). The complex PW 12/FSM-16 (m) was characterized by IR, XRD, spectrum NMR and CV. The results show the framework of FSM-16 is retained upon inserting the guest compound and the composite is an active electrocatalyst for the reduction of NO 2 −.
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