Abstract
In the crystal structure of the title compound, C9H13N3S, molecules are linked through N—H⋯S and N—H⋯N hydrogen bonds, forming hydrogen-bonded tapes along the b axis. The dihedral angle between the phenyl ring and the thiourea group is 44.9 (2)°.
Highlights
In the crystal structure of the title compound, C9H13N3S, molecules are linked through N—HÁ Á ÁS and N—HÁ Á ÁN hydrogen bonds, forming hydrogen-bonded tapes along the b axis
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: FY2013)
R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger
Summary
Key indicators: single-crystal X-ray study; T = 173 K; mean (C–C) = 0.002 A; R factor = 0.033; wR factor = 0.088; data-to-parameter ratio = 17.6. In the crystal structure of the title compound, C9H13N3S, molecules are linked through N—HÁ Á ÁS and N—HÁ Á ÁN hydrogen bonds, forming hydrogen-bonded tapes along the b axis. The dihedral angle between the phenyl ring and the thiourea group is 44.9 (2). Related literature For the synthesis of the title compund, see: Lee et al (1985). See: Tommasino et al (1999, 2000); Leung et al (2008). See: Guo (2007); Okino et al (2005)
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