Abstract
An electrochemical process to synthesize stannous fluoborate by means of ion-exchange membranes was established. The anodic limiting current could reach 6 A dm−2 and the current efficiency was over 95%. A galvanostatic method was adopted to study the kinetics of anodic dissolution of tin in fluoboric acid. The exchange current density was evaluated to be 4.57 mA dm−2. Polarographic study of the cathodic reaction of stannous ions also confirmed that the process was diffusion controlled.
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