Abstract

Flash Vacuum Thermolysis of 1,5-bis-(1-chloroethenyl)anthracene (6) gives cyclopent[hi]-aceanthrylene (2) which at T≥9000 °C rearranges to cyclopent[hi]acephenanthrylene (1). This conversion occurs more readily than that of the monocyclopenta-fused aceanthrylene to acephenanthrylene.

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