Abstract
High-angular-resolution powder-diffraction-experiments for the crystal structure analysis using synchrotron radiation are described. Topics discussed in this chapter are: 1) long horizontal parallel slits and crystal analyzer, 2) the accurate measurement of unit-cell parameters in the p.p.m. order, 3) the multiple-detector system for powder diffractometer and 4) the high-angular-resolution diffraction data and the accuracy of crystal structure analysis.
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