분말 혼합 공정으로 만들어진 은계 삽입금속의 특성

Abstract

Ag계 분말 삽입금속을 볼 밀링법으로 제조하였다. 밀링공정의 변수들은 밀링시간을 제외하고는 일정하게 하였고 밀링 시간은 24, 48, 72시간들로 정하였다. 밀링에 의해 제조된 삽입금속들은 SEM관찰, DSC분석, 퍼짐성, 젖음성 시험을 통해 평가하였다. 삽입금속들의 브레이징부 특성은 상용금속에 비하여 우수하였다. 48시간 동안 밀링한 삽입금속이 퍼짐성과 젖음 특성이 가장 우수한 조건임을 나타냈다. 또한 브레이징부는 작은 양의 기공을 포함하고 있지만 안정적인 미세조직을 보였고 미세경도는 138VHN으로 나타났다. 【Powder type Ag system insert metals were manufactured by ball milling process. The variables of milling process were constant except the milling time. The milling times were selected for 24, 48 and 72 hours. The insert metals made by milling process were evaluated by performing scanning electron microscope, DSC(differential scanning calorimetry) analyses, spreading test and further in terms of wettability test. The selected insert metals that have the good characteristics compared to commercial insert metals were applied to make the brazed joints. The characterizations of those brazed joints were also conducted by microstructural observations. The results indicated that milling time of 48 hours for making powder type insert metals was the best condition showing the good spreadibility, low wetting angle. The brazed joints that applied the 48 hours milled insert metal were very sound condition indicating the stable microstructure in spite of containing small amount of porosity and the microhardness value of the joint was about 138VHN.】