A 5 MHz ultrasonic transducer transmission method was used to study recovery processes subsequent to plastic deformation in a polycrystalline, high purity iron-0.05% carbon alloy. Simultaneous and continuous measurements were made of stress relaxation and attenuation recovery in the temperature range 77° K < T < 300° K. Below about 180°K, the effect of interstitial pinning of dislocations was Found to be negligible. Above this temperature, interstitial pinning was found to be a two-stage thermally activated process with a time exponent of 2 3 in the first stage, changing to 1 2 in the second. The activation energy of the first stage was determined as 12.5 kcal/mole by a Granato-Hikata-Lücke analysis and as 11 kcal/mole by an Arrhenius analysis of the time to transition from the first to the second stage. It is argued that for the first stage these values are consistent with Schoeck and Seeger re-organization of carbon interstitials about strain induced screw dislocations. The second stage is believed to be Cottrell-Bilby bulk diffusion toward the dislocations.
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