Texturing Process Research Articles

An analytical cutting force model for elliptical vibration texturing of nano-grating surfaces

Although the direct texturing processes using dynamic cutting depth modulation have been widely demonstrated for generating micro/nano-structured surfaces, the material shearing removal dominates the surface topography generation that inevitably inhibits the machining feasibility of high-aspect textures. This paper proposes a novel nano-grating generation mechanism governed by the combined effect of shearing-based material removal and compressive forming-based deformation in elliptical vibration texturing. A newly dynamic cutting force model is established to reveal its transient cutting mechanics that incorporating the process elastic rebounding behaviors and essential local cutting characteristics in three deformation zones. The model fully considers the complex transient shear angle variation, friction reversal phenomenon on tool-chip interface as well as the unique flank-waviness interaction. A series of texturing experiments are delicately designed to modulate the contribution of material shearing removal and flank compressive forming on nano-grating generation mechanism. The measured dynamic cutting force show good agreements with the simulated results, based on which the model accuracy and main process assumptions are well validated. Furthermore, the relationship between the cutting force characteristics and nano-grating topography is analyzed to guide the optimal elliptical trajectory designs for simultaneously achieving high-quality nano-gratings and smaller dynamic cutting forces. The outcomes of this paper not only lay the scientific foundations for machining capability extension of direct texturing processes, but also contribute to the understandings of combined surface generation mechanisms of other intermittent cutting processes in nano-scale domain.

Development of a protein food based on texturized wheat proteins, with high protein digestibility and improved lysine content

The development of plant-based protein foods may facilitate the decrease in animal product consumption in western countries. Wheat proteins, as a starch coproduct, are available in large amounts and are good candidates for this development. We investigated the effect of a new texturing process on wheat protein digestibility and implemented strategies aimed at enhancing the lysine content of the product developed. Protein true ileal digestibility (TID) was determined in minipigs. In a preliminary experiment, the TID of wheat protein (WP), texturized wheat protein (TWP), TWP enriched with free lysine (TWP-L), or with chickpea flour (TWP-CP) was measured and compared to beef meat proteins. In the main experiment, minipigs (n = 6) were fed a dish (blanquette type) containing 40 g of protein in the form of TWP-CP, TWP-CP enriched with free lysine TWP-CP+L, chicken filet, or texturized soy, together with quinoa (18.5 g of protein) in order to improve meal supply of lysine. Wheat protein texturing did not affect total amino acid TID (96.8 % for TWP vs 95.3 % for WP), which was not different from that of beef meat (95.8 %). Chickpea addition did not affect protein TID (96.5 % for TWP-CP vs 96.8 % for TWP). The Digestible Indispensable Amino Acid Score for adults of the dish combining TWP-CP+L with quinoa was 91, whereas it was 110 and 111 for the dishes containing chicken filet or texturized soy. The above results show that, by optimizing lysine content through the formulation of the product, wheat protein texturization can enable the development of protein-rich products of nutritional quality compatible with quality protein intake in the context of a complete meal.

Investigation of the influence of the processing speed and the linear pulse density of the laser surface texturing process

Fine-tuning laser parameters is necessary to achieve the desired quality of the process of laser surface texturing. This requires a set of experiments to assess the influence of the main process parameters on the quality of the surface of a treated alloy. By varying the laser parameters, different laser-material interactions, such as heating, melting, or evaporation can be observed. This study analyzes the influence of two interrelated processing parameters in laser surface texturing – the speed of beam motion on the surface on the one hand, and, on the other, the linear pulse density. They ultimately have a direct impact on the resulting microstructure, hydrophilicity, and electrochemical properties of austenitic steel (AISI 304). By adjusting the pulse repetition rate of a 1064-nm fiber laser from 500 kHz to 1000 kHz at a constant speed of 100 mm/s, the surface wettability changes from hydrophobicity to hydrophilicity. All surfaces treated with laser scanning speeds varying from 20 mm/s to 200 mm/s at a constant rate of 500 kHz are hydrophobic. As a result, the changed ability to repel liquids alters the corrosion properties of the steel in a 0.5 M H2SO4 solution. The results allow one to distinguish ranges of laser-beam parameters that could be useful in selecting certain properties of the stainless-steel surface layer.

Optically‐Boosted Planar IBC Solar Cells with Electrically‐Harmless Photonic Nanocoatings

AbstractAdvanced light management via front‐coated photonic nanostructures is a promising strategy to enhance photovoltaic (PV) efficiency through wave‐optical light‐trapping (LT) effects, avoiding the conventional texturing processes that induce the degradation of electrical performance due to increased carrier recombination. Titanium dioxide (TiO2) honeycomb arrays with different geometry are engineered through a highly‐scalable colloidal lithography method on flat crystalline silicon (c‐Si) wafers and tested on standard planar c‐Si interdigitated back‐contact solar cells (pIBCSCs). The photonic‐structured wafers achieve an optical photocurrent of 36.6 mA cm−2, mainly due to a broad anti‐reflection effect from the 693 nm thick nanostructured coatings. In contrast, the pIBCSC test devices reach 14% efficiency with 679 nm thick TiO2 nanostructures, corresponding to a ≈30% efficiency gain relative to uncoated pIBCSCs. In addition, several designed structures show unmatched angular acceptance enhancements in efficiency (up to 63% gain) and photocurrent density (up to 68% gain). The high‐performing (yet electrically harmless) LT scheme, here presented, entails an up‐and‐coming alternative to conventional texturing for c‐Si technological improvement that can be straightforwardly integrated into the established PV industry.

Beef and plant-based burgers' mastication parameters depend on texture rather than on serving conditions.

Previous studies dealing with plant-based meat analogs confirmed the potential of oral processing methods to identify options for improving those products. Knowing that sensory perception can be influenced by adding condiments, this short communication aimed to investigate the texture and oral processing of four plant-based burger analogs and a beef burger when consumed in portions or as part of model meals with buns and sides. Texture profile analysis indicated that beef burgers and analog E were the toughest. Two analogs (B and S) showed textures close to beef, while one (analog D) displayed significantly lower values for hardness, toughness, cohesiveness, and springiness. The instrumental data was only partly reflected in the mastication parameters. Adaptations in mastication behavior were expected, but differences between the plant-based analogs were smaller than anticipated, although clear differences were observed for consumption time, number of chews and number of swallows. On the whole, mastication patterns concurred within different consumption scenarios (portions, model burgers), and significant correlations with instrumental texture were obtained.

Spatial antiferromagnetic spin texture as a nano-oscillator

We report a theoretical study of the localized spatial magnetization configuration, which is a confined spin configuration of the target skyrmion/hopfion type in an antiferromagnet with perpendicular magnetic anisotropy, and then we solve the particular problem of self-oscillations of such a topological spin texture. Using the energy approach, a self-consistent account of inhomogeneity of the characteristics of the topological magnetic spin texture was carried out. On this basis, the equation of free oscillations of the confined spin configuration magnetization was derived and its quasi-classical solution was found. For a thin ring spin texture, the frequency, period of oscillations and relative amplitude of the main tone of oscillations are found. For the first time, we determined the topological mass, inertial mass and total energy of the main tone of oscillations of such spatial spin texture. The self-oscillatory process of a spatial spin texture is interpreted as a magnetic nano-oscillator.

Effect of Wheat Gluten and Peanut Protein Ratio on the Moisture Distribution and Textural Quality of High-Moisture Extruded Meat Analogs from an Extruder Response Perspective.

Wheat gluten (WG) and peanut protein powder (PPP) mixtures were extruded at high moisture to investigate the potential application of this mixture in meat analog production. Multiple factors, including the water absorption index (WAI), water solubility index (WSI), rheological properties of the mixed raw materials, die pressure, torque and specific mechanical energy (SME) during high moisture extrusion, texture properties, color, water distribution, and water activity of extrudates were analyzed to determine the relationships among the raw material characteristics, extruder response parameters, and extrudate quality. At a WG ratio of 50%, the extrudates have the lowest hardness (2.76 kg), the highest springiness (0.95), and a fibrous degree of up to 1.75. The addition of WG caused a significant rightward shift in the relaxation time of hydrogen protons in the extrudates, representing increased water mobility and water activity. A ratio of 50:50 gave the smallest total color difference (ΔE) (about 18.12). When the added amount of WG was 50% or less, it improved the lightness and reduced the ΔE compared to >50% WG. Therefore, clarifying the relationship among raw material characteristics, extruder response parameters, and extruded product quality is helpful in the systematic understanding and regulation of the fiber textural process of binary protein meat analogs.

Influence of pulsed Nd:YAG laser oscillation energy on silicon wafer texturing for enhanced absorption in photovoltaic cells

The influence of the Nd:YAG laser's oscillation energy on creating textured surfaces on silicon wafers is investigated in this study. The silicon wafer surfaces were directly ablated by a pulsed Nd:YAG laser beam to create the texturing, which was then examined using UV–Vis spectroscopy, AFM andFESEM to determine its characteristics. The reflectance was reduced up to 15% after laser texturing of multicrystalline silicon wafers. The silicon surface suffers from structural defects and a laser damage layer as a result of the laser texturing process, which in turn has an effect on the lifespan of the photo-generated carriers. To compensate for the laser damage layer, the silicon surface was cleaned with diluted KOH (15%) to remove undesirable particles and the oxide layer. Surface roughness and reflectance in silicon solar cells were changed depending on the laser oscillation energy utilized for texturing. The roughness and reflectance were measured using AFM and UV–Vis, respectively. The laser oscillation energy of 84 J/p had the highest average roughness of 0.2104 m and the lowest reflectance of 5%. As a result, standardsilicon solar cell devices revealed photovoltaic conversion efficiencies of roughly 7.5% and 5.0% for laser-textured grid and one-dimensional line patterns, respectively.

Lead zirconate titanate ceramics with aligned crystallite grains.

The piezoelectric properties of lead zirconate titanate [Pb(Zr,Ti)O3 or PZT] ceramics could be enhanced by fabricating textured ceramics that would align the crystal grains along specific orientations. We present a seed-passivated texturing process to fabricate textured PZT ceramics by using newly developed Ba(Zr,Ti)O3 microplatelet templates. This process not only ensures the template-induced grain growth in titanium-rich PZT layers but also facilitates desired composition through interlayer diffusion of zirconium and titanium. We successfully prepared textured PZT ceramics with outstanding properties, including Curie temperatures of 360°C, piezoelectric coefficients d33 of 760 picocoulombs per newton and g33 of 100 millivolt meters per newton, and electromechanical couplings k33 of 0.85. This study addresses the challenge of fabricating textured rhombohedral PZT ceramics by suppressing the otherwise severe chemical reaction between PZT powder and titanate templates.

Affective topologies and virtual tactile experiences in theatre training

My experience as a performer is largely informed by my long-term connection with the Bridge of Winds group, led by Iben Nagel Rasmussen. As a practitioner-researcher however, I am engaged on a new journey, where my embodied knowledge is guiding the construction of a virtual archive for theatre practices. During this process, one of the main issues we are facing is that of renegotiating the sense of touch in virtual spaces. As the refined tactile feedback from my masters has taught me to reconnect with the present continuously; is it possible to create this sense of learning via interactive, virtually designed spaces? While aiming at building an immersive space which one can train in and with, what tactics can we imagine to evoke touch-like experiences of force, weight, pressure, connection and above all, care? Furthermore, can such spaces shift the boundaries of what we might understand as touch? These writings are informed by an experiment which translates Odin actress Roberta Carreri’s workshop Dance of Intentions into a virtual archive. Whilst critically approaching this textural translation process and raising the social-political implications of such translations, I will suggest ways in which designed immersive environments can renegotiate tactile experiences in theatre training.

Pose-Driven Realistic 2-D Motion Synthesis.

A realistic 2-D motion can be treated as a deforming process of an individual appearance texture driven by a sequence of human poses. In this article, we thereby propose to transform the 2-D motion synthesis into a pose conditioned realistic motion image generation task considering the promising performance of pose estimation technology and generative adversarial nets (GANs). However, the problem is that GAN is only suitable to do the region-aligned image translation task while motion synthesis involves a large number of spatial deformations. To avoid this drawback, we design a two-step and multistream network architecture. First, we train a special GAN to generate the body segment images with given poses in step-I. Then in step-II, we input the body segment images as well as the poses into the multistream network so that it only needs to generate the textures in each aligned body region. Besides, we provide a real face as another input of the network to improve the face details of the generated motion image. The synthesized results with realism and sharp details on four training sets demonstrate the effectiveness of the proposed model.

Generating micro/nanostructures on magnesium alloy surface using ultraprecision diamond surface texturing process

The lightness and high strength-to-weight ratio of the magnesium alloy have attracted more interest in various applications. However, micro/nanostructure generation on their surfaces remains a challenge due to the flammability and ignition. Motivated by this, this study proposed a machining process, named the ultraprecision diamond surface texturing process, to machine the micro/nanostructures on magnesium alloy surfaces. Experimental results showed the various microstructures and sawtooth-shaped nanostructures were successfully generated on the AZ31B magnesium alloy surfaces, demonstrating the effectiveness of this proposed machining process. Furthermore, sawtooth-shaped nanostructures had the function of inducing the optical effect and generating different colors on workpiece surfaces. The colorful letter and colorful flower image were clearly viewed on magnesium alloy surfaces. The corresponding cutting force, chip morphology, and tool wear were systematically investigated to understand the machining mechanism of micro/nanostructures on magnesium alloy surfaces. The proposed machining process can further improve the performances of the magnesium alloy and extend its functions to other fields, such as optics.

The effect of laser surface textures on the adhesion strength and corrosion protection of organic coatings - Experimental assessment using the pull-off test and the shaft load blister test

Adhesion is necessary for an effective corrosion protection of metallic surfaces through organic coatings. Even the best anticorrosive coatings fail if it is not well adhered to the substrate. Laser surface texturing (LST) process has been widely used for enhancing adhesion between coatings and steel surfaces in various applications. In addition, recent researches have proven that LST is an effective option for pretreatment of steel surfaces prior to organic coating deposition. This work reports an investigation on the adhesion strength of organic coatings deposited onto AISI-A36 carbon steel laser-textured surfaces. Nanosecond LST via the direct laser writing (DLW) method was used to fabricate V-shaped grooves on the steel surfaces. The distance between consecutive grooves was varied to obtain different surface topographies with controlled surface textured area (TA) ranging from 10 % to 60 %. Conventional bead-blasted surfaces were used as a reference. Surface morphology and topography were characterized through roughness and tortuosity. The frequently used pull-off test (ISO 4624) and a shaft load blister test (SLBT) were used to determine the adhesion of the epoxy coating. In addition, accelerated corrosion tests were carried out to assess the effects of the laser textured surface conditions on the corrosion propagation. After running the pull-off test, all the surfaces' conditions exceeded the minimum pull-off strength value of 5 MPa stated in ISO 12944-9. The results for the SLBT showed that the adhesive strength is highly influenced by the laser-textured area. The geometrical aspects of the groove structure promote phenomena such as mechanical interlock and mechanical hooking of the coating, which affect the adhesion failure mechanism of the organic coating during the test. For lower TA, the crack propagation occurs mainly at the coating/steel interface. However, increasing the TA shows that the crack propagation is stopped near the V-shaped grooves due to the complex shape and must deviate inside the coating for further propagation. Finally, adhesion strength results were correlated with coating delamination rates and an indirect relationship was found.

Study on the Matching of Surface Texture Parameters and Processing Parameters of Coated Cemented Carbide Tools

Placing micro-textures on a tool surface can play an anti-wear and friction-reducing role and capture impurities and improve the tool-chip friction state, thus improving the cutting performance of the tool and the quality of the workpiece. To ensure the processing quality in the micro-texture-coated tool-cutting process, the process parameters and micro-texture parameters are limited to smaller parameters, which reduces the processing efficiency and increases the cost. Aiming at this problem, this paper designs orthogonal experiments of the cutting process and micro-texture parameters, builds an experimental platform for milling titanium alloy with a micro-texture-coated ball-end milling cutter, analyzes the influence of cutting parameters on tool milling performance and workpiece quality, establishes a high fitting prediction model, and optimizes parameters. The results show that the cutting parameters significantly affect the milling force, tool wear, and workpiece surface roughness, which are in the first response level, and the micro-texture parameters, which are in the second response level. It is proven that micro-texture has anti-wear and anti-friction effects, and it is found that micro-texture parameters affect the evaluation index by changing the distribution state of the micro-texture. It is found that the multiple linear regression model fits better. Parameter optimization results are: v = 159.4232 (m/min), ap = 0.211 (mm), f = 0.06 (mm/r), micro-pit diameter D = 62.3429 (μm), distance from blade L = 121.5184 (μm), and micro-pit spacing L1 = 235.6443 (μm). It provides some guidance for the selection of micro-texture parameters and cutting parameters on a micro-texture-coated tool.

Effect of Femtosecond Laser Processing Parameters on the Ablation Microgrooves of RB-SiC Composites

Because of the high hardness, brittleness, and anisotropy of reaction-bonded silicon carbide composites (RB-SiC), it is challenging to process high-quality textures on their surfaces. With the advantages of high processing accuracy and low processing damage, femtosecond laser processing is the preferred technology for the precision processing of difficult-to-process materials. The present work used a femtosecond laser with a linear scanning path and a spot diameter of 18 µm to process microgrooves on RB-SiC. The influence of different processing parameters on the microgroove profile, dimensions, and ablation rate (AR) was investigated. The ablation width Wa and average ablation depth Da of microgrooves were evaluated, and the various patterns of varying processing parameters were obtained. A model for Wa prediction was developed based on the laser fluence within the finite length (FL). As a result, the experimental values were distributed near the prediction curve with a maximum error of 20.4%, showing an upward trend of gradually decreasing increments. For a single pass, the AR value was mainly determined by the laser energy, which could reach the scale of 106 μm3/s when the laser energy was greater than 50 μJ. For multiple passes, the AR value decreased as the number of passes increased and it finally stabilized. The above research will provide theoretical and experimental support for the high-quality and efficient processing of RB-SiC surface textures.

Ultrashort Laser Texturing of Superelastic NiTi: Effect of Laser Power and Scanning Speed on Surface Morphology, Composition and Wettability

Among metallic biomaterials, near-equiatomic NiTi is one of the most promising intermetallic system applicable for biomedical applications, thanks to its high biocompatibility and unique superelasticity (or pseudoelasticity), offering a complete recoverable strain up to 8%. In the prospective uses for bio-devices, the surface processing of NiTi medical components plays a fundamental role for guaranteeing both a Ti oxide passivizing layer for avoiding Ni ion release into the human body and surface morphology for controlling the cell proliferation. Mechanical polishing, thermal, chemical or electro-chemical treatments are typically performed for surface modifications. Recently, laser texturing has been successfully applied for different materials, included NiTi shape memory alloys, and also for tuning the surface properties, such as wettability. In the present work, ultrashort laser surface modification was carried out, through the use of a femtosecond laser, for the surface texturing of commercial superelastic NiTi plates. The main goal is to investigate the correlation among morphology, chemical composition and wettability with the principal process parameters, such as average power and scanning velocity in high power ultrashort laser texturing. Laser patterned surfaces were characterized by means of scanning electron microscopy, 3D-profilometry, XPS analysis and wetting measurements. After the laser treatments, both surface morphology and Ni/Ti ratio were largely modified from the initial surface, depending on the adopted process parameters. The wettability of the laser textured surfaces can be also varied with respect to the initial surface, due to the roughness values and grooves induced by the laser beam scans. The laser texturing process induced a combination between micro and nano structures, depending on the input energy. In details, the surfaces were tuned to lower roughness values (from 0.4 μm to 0.3 μm) with a laser power of 1 W, while it was increased up to 0.65 μm with a laser power of 13 W. The laser surface modification promoted a change of the contact angle from 70° of the untreated condition up to 135° to the surface laser treated with a power of 13 W.

Tailoring tribological properties of Ti-Zr alloys via process design of laser surface texturing and thermal oxidation

The optimization of texture density and processing sequence of duplex-treatment of thermal oxidation (TO) and laser surface texturing (LST) were studied to maximize the tribological performance of titanium alloys. The tribological properties of the samples were investigated under starved lubrication, and compared with TO-only sample. The results show that compared to TO-only sample, all the duplex-treatment can reduce the friction coefficient and wear rate. The samples with a surface density of 10% show excellent tribological performance regardless of the processing sequence. Fe2O3 was formed and adhered to the worn surfaces of the discs in the process of wear due to the wear of the counterpart ball. The higher surface density could lead to the enhanced destruction and adhesive wear of the surface.

Improvement of Frictional Property of AISI D2 Tool Steel Surface against JIS SPFC 980Y Advanced High-Strength Steel by Using Laser Texturing Process

Surface friction in metal forming processes can be reduced by creating lubricant reservoirs at the interface between surfaces in contact, and a laser texturing process can be employed to produce the micro-dimples that act as the reservoirs on the surfaces. However, the role of the laser texturing parameters in the friction reduction of tool steel surfaces has still received very little attention. Therefore, this study aims to reduce the friction of the AISI D2 tool steel surface on which a nanosecond pulse laser was applied to create an array of micro-lubricant pockets for trapping lubricant. The effects of laser power, irradiation duration, and spacing distance between pockets on the pocket diameter, size of the heat-affected zone, surface friction, and wettability were investigated in this work. The average laser power in the range from 5 to 10 W and laser irradiation duration of 0.02 to 0.10 s were applied. The results showed that the increase in laser power and irradiation duration enlarged the pocket diameter and heat-affected zone. The largest pocket diameter of 40 µm was achievable by using 10 W laser power together with 0.10 s irradiation time. The pin-on-disc method was employed to determine the friction coefficient of the tool steel, where JIS SPFC 980Y advanced high-strength steel was used as a disc. The friction coefficient of laser-textured with different spacing distances of 150, 200, and 250 µm versus untextured surfaces was compared and found to vary depending on the applied normal load. The laser-textured surface having a pocket spacing distance of 150 µm and pocket density of 5.6%, offered the lowest friction coefficient of 0.097 on average for all tested loads, whereas the average friction coefficient of the untextured surface was 0.117. In addition, the wettability of textured surfaces was insignificantly changed compared to that of untextured ones, so the micro-lubricant pockets did not cause oleophobicity affecting the performance of lubrication. Well-defined micro-pockets using the most appropriate laser parameters, i.e., 10 W laser power with 0.10 s irradiation duration and 150 µm spacing distance, successfully reduced the sliding friction of contacting couples between the laser-textured tool steel and advanced high-strength steel surfaces. The low surface friction induced by the laser-fabricated micro-lubricant pockets has been feasible for the forming tool and die applications where the energy consumed in their operations can be minimized.

Morphological and Optical Study of Black P- Silicon Textured in KOH Bath

This paper reports the temperature and the concentration dependence of anisotropic etching for (100) p-Silicon in an aqueous KOH solution etching rate of wet etching has been experimentally determined with varying concentrations and the temperature of the KOH solution. The texturing process was managed at different etching durations ( 20 min, 40 min, and 60 min). XRD test showed that the lowest value of grain size was 5.0 nm (obtained with the highest porosity percentage of 50% with 4.5% KOH concentration for 60 min). FESEM test showed that the pore diameter increased with increasing etching time. The lowest reflectance value was (2.8 % at 550 nm wavelengths for samples treated with 4.5% KOH concentration for 60 min etching time. The refractive index value was 1.8 for the same black Si sample, also Hall test is introduced.

Comparison of in vitro digestibility and DIAAR between vegan and meat burgers before and after grilling

Plant-based meat alternatives of high quality and digestibility could be a way to reduce meat consumption and, consequently, the environmental impact. However, little is known about their nutritional characteristics and digestion behaviour. Therefore, in the present study, the protein quality of beef burgers, known as excellent source of protein, was compared with the protein quality of two highly transformed veggie burgers, based on soy or pea-faba proteins, respectively. The different burgers were digested according to the INFOGEST in vitro digestion protocol. After digestion, total protein digestibility was determined, either based on total nitrogen (Kjeldahl) analysis, or after acid hydrolysis based on total amino groups (o-phthalaldehyde method) or total amino acids (TAA; by HPLC). The digestibility of individual amino acids was also determined, and the digestible indispensable amino acid score (DIAAS) was calculated based on in vitro digestibility. The impact of texturising and grilling on in vitro protein digestibility and the digestible indispensable amino acid ratio (DIAAR) was evaluated at the level of the ingredients and the finished products. As expected, the grilled beef burger had the highest in vitro DIAAS values (Leu 124 %), and grilled soy protein-based burger reached in vitro DIAAS values that could be rated as good (soy burger, SAA 94 %) protein source, according to the Food and Agriculture Organization. The texturing process did not significantly affect the total protein digestibility of the ingredients. However, grilling led to a decrease in digestibility and DIAAR of the pea-faba burger (P < 0.05), which was not observed in the soy burger, but led to an increase in DIAAR in the beef burger (P < 0.005).