Shear Bond Strength Measurements Research Articles

Shear bond strength between dental adhesive systems and an experimental niobium-based implant material

This study aimed to investigate adhesive shear bond strength (SBS) on an ultrafine-grained niobium alloy (UFG-Nb) that is a potential dental implant material. SBS of three adhesive systems combined with three composites to UFG-Nb was compared to corresponding SBS to Ti-6Al-4V and to zirconia. Specimens of the substrates UFG-Nb, Ti-6Al-4V and zirconia with plane surfaces were sandblasted with Al2O3, cleaned and dried. Three adhesive systems (Futurabond U, Futurabond M + , Futurabond M + DCA; all VOCO GmbH, Cuxhaven, Germany) were applied each on specimens of each substrate and light cured. One composite (BifixSE, BifixQM, GrandioSO; all VOCO GmbH) was applied and light cured resulting in 27 groups (n = 10) for all substrate-adhesive-composite-combinations. SBS was measured after 24 h of storage. To simulate aging equally prepared specimens underwent 5000 thermocycles before SBS measurement. There was no significant difference in SBS within the non-aged groups. Among the artificially aged groups, GrandioSO-groups showed a greater variance of SBS than the other composites. All significant differences of corresponding UFG-Nb-, Ti-6Al-4V- and zirconia-groups with same adhesive-composite-combination (ACC) were observed between UFG-Nb and zirconia or Ti-6Al-4V and zirconia but never between the two metallic substrates. The similarity between these materials might show in their adhesive bonding behavior. As there were no differences comparing corresponding groups prior to and after artificial aging, it can be concluded that aging does not affect SBS to UFG-Nb, Ti-6Al-4V and zirconia using the tested ACCs. Adhesive bonding of established ACCs to UFG-Nb is possible resulting in SBS comparable to those on Ti-6Al-4V and zirconia surfaces.Graphical

Shelf-life effect of silane-containing universal adhesive on bonding effectiveness to glass-ceramic

ObjectiveTo evaluate the shelf-life effect of a silane-containing universal adhesive (UA) on its shear bond strength (SBS) to lithium disilicate glass-ceramic (LiSi2). MethodsSBS to mirror-polished (‘MP’) and hydrofluoric acid-etched ground (‘HF’) lithium disilicate glass-ceramic (Initial LiSi, GC) with/without prior separate ceramic primer application (G-Multi Primer, GC: ‘G-MP’) was measured. Scotchbond Universal Plus (‘SBUp’) (3M Oral Care) was used 33 (‘fresh’) and 6 (‘expiring’) months before the expiration date. ‘MP’ specimen preparation involved (1) ‘G-MP’ priming (or not), (2) ‘SBUp’ application, (3) composite (Clearfil AP-X, Kuraray Noritake) placement, and (4) 20 s light-curing (SmartLite Pro, Dentsply Sirona). ‘HF’ specimen preparation involved (1) HF (Porcelain Etch, Ultradent) etching, (2) phosphoric acid (K-Etchant, Kuraray Noritake) post-etching, with (3) and (4) being the same as for ‘MP’. Upon light-curing, all specimens were stored in 37 °C water for either 1 week (‘immediate’) or 3 months (‘aged’) prior to SBS measurement. Statistics involved Linear Mixed-Effects modelling (α = 0.05). ResultsSBS was not significantly affected by SBUp's shelf life, except for a significantly higher SBS recorded for ‘fresh’ SBUp applied on HF-etched and separately silane-primed LiSi2. Aging did not significantly decrease SBS. In fact, a significant increase in SBS upon aging was recorded for HF-etched LiSi2 that was not separately silane-primed. The significantly highest bond strength was measured when LiSi2 was HF-etched followed by separate silane-priming. SignificanceDespite the UA investigated has silane in its formulation, the most effective and durable bonding to LiSi2 was achieved by HF-etching followed by separate silane-priming, irrespective of the UA's shelf life.

The Effect of Nano Hydroxyapatite on the Bond Strength of Acrylic Teeth Repaired to an Acrylic Resin Denture Base Using Two Types of Auto Polymerized Acrylic Resins

The insufficiently binder between acrylic teeth and dentures is considered to be the primary cause of teeth fractures from the dentures and is one of the disadvantages of acrylic denture base material. This research has been conducted to assess various concentrations of Nano hydroxyapatite addition on the shear bond between repaired acrylic teeth and polymer. One-hundred specimens of resin were split into two main subdivisions. 50 specimens were repaired with cold cured Duracryl Plus and the other 50 were repaired with a special type of acrylic O-cry1. Each one was sectioned into tested groups depending on (1%., 2%., 3%, and 5% by wt. of nano hydroxyapatite) incorporation and control group (0% of nano hydroxyapatite) with (n=10). The Universal testing machine was utilized for shear bond strength measurement. The obtained values were diffracted by t-test, ANOVA, and LSD-test. There was an increase in bond strength that repairing with O-cry1 than Duracryl Plus with a heightening in the bond strength, which was seen with incorporating nano hydroxyapatite into the acrylic resin with a significant difference between them. The 2% wt. Nano hydroxyapatite group demonstrated the maximum mean values, while those for the 5% wt. Nano hydroxyapatite group were recording minimum value with a significant difference between them. Repairing with O-cry1 recording better bond strength than Duracryl Plus acrylic. Furthermore, the addition of hydroxyapatite in Nano-form has successfully improved the “shear bond strength” of teeth to the PMMA at 2% wt. nano hydroxyapatite.

Debonding of LDSVs utilising Er,Cr:YSGG laser irradiation with fractional technique: an in vitro study.

The removal of porcelain laminate veneers with rotary instruments could be accompanied by microfractures because differentiation of the veneer from the dental structure and resin cement is not a highly selective procedure. This can lead to scratches and overheating of the enamel and patient discomfort. Therefore, this in vitro research aimed to examine the effectiveness of the 2790 nm Er,Cr:YSGG laser utilizing a fractional technique to debond lithium disilicate veneer. Six groups of 30 extracted permanent bovine mandibular incisors were selected. Twenty-five samples, G1-5, (n = 5) laser-irradiated groups, and the last five samples (C) were considered the control group. The tested groups were irradiated with 3-5 W output power of Er,Cr:YSGG laser for time intervals of 50 s. During irradiation, the temperature in the pulp chamber was monitored using a thermocouple connected to a digital multilogger thermometer inside the sample's pulp chamber. Subsequently, the shear bond strength was measured for all groups. Furthermore, the remaining adhesive index was measured using a stereomicroscope, the area was analysed, and then transformed into scores. Finally, one untreated sample and two samples of the highest power value from laser-treated groups were examined using a scanning electron microscope (SEM) for their surface morphology. All debonding protocols were safe regarding intrapulpal temperature increment. The highest temperature elevation was recorded at 5 W, which increased by 1.7 °C. Considering the shear bond strength measurement, there was a significant reduction after laser irradiation for G1-5 compared with group C. Er,Cr:YSGG laser with a fractional technique can be used successfully for veneer removal. Besides safe temperature rising, veneers can be reused because there was neither a fractured specimen during the whole study nor major irregularities or cracks shown in SEM pictures analysis for the veneer surfaces; thus, they can be removed quickly, safely, and comfortably using Er,Cr:YSGG. © 2023 Australian Dental Association.

Effectiveness of surface polishing after debonding of metal brackets from different CAD-CAM materials.

The purposes of this study were to compare and evaluate the surface texture of different restorative computer-aided design and computer-aided manufacturing (CAD/CAM) materials before bonding and after debonding of metal orthodontic brackets. Atotal of 60rectangular ceramic test specimens (n = 20 in each group) were prepared using feldspathic ceramic blocks (FLD; served as control), hybrid ceramic blocks (HC), and lithium disilicate ceramic blocks (LDC). Surface roughness (Ra) analysis was conducted using aprofilometer before bonding the metal brackets. After the debonding and polishing procedures, asecond surface roughness analysis was conducted on each specimen. The shear bond strength (SBS) test was applied to each specimen using auniversal test machine for debonding the metal brackets. The debonded specimens were examined under astereomicroscope and scored using a4-step adhesive remnant index (ARI). The Ra and SBS values and the ARI scores were saved, and the data were analyzed statistically at asignificance level of 0.05. One specimen from each group was examined under atomic force microscopy to visualize surface roughness. Furthermore, one specimen from each group was additionally prepared for scanning electron microscopy analysis. Statistically significant differences in SBS measurements were observed between all three groups. The highest SBS values were obtained from the FLD group, the lowest from the LDC group. The HC group showed significantly (P = 0.001) lower Ra values than the LDC and FLD groups after debonding and polishing. No significant differences were observed in the ARI scores between the groups. Hybrid ceramics could be asuitable alternative for fixed restorations in adult patients receiving subsequent treatments with fixed orthodontic appliances.

The effect of mechanical and chemo-mechanical temporary cement cleaning methods on shear bond strength with self-adhesive resin cement (an in-vitro study)

BackgroundAdhesive tooth-colored restorations are strongly dependent on the substrate surface cleanliness to allow intimate contact between resin cement and dentin surface, so several methods were adopted for the total cleaning of temporary cement residues. This study aimed to assess the effect of mechanical and chemo-mechanical cleaning methods of temporary cement on the immediate shear bond strength of self-adhesive resin cement to dentin surface.MethodsForty freshly extracted lower first premolars were cut to expose a flat dentin surface. Discs of temporary crown composite resin material were constructed and cemented to the flat dentin surface using resin-based and non-eugenol temporary cement then stored at room temperature in distilled water. Dividing of samples into two groups according to the method of temporary cement cleaning. Group I (n = 20) mechanical cleaning using the rotary instrument, and group II (n = 20) chemo-mechanical cleaning using chlorhexidine-containing scrub. CAD/CAM reinforced Composite discs were bonded to the dentin surface using self-adhesive composite resin cement, then measurement of shear bond strength was done using a universal testing machine. Further analysis of failure mode after debonding was performed by Scanning electron microscope.ResultsNo statistically significant difference was found between the mean shear bond strength of the two cleaning methods (P-value = 0.636). Regardless of the cleaning method, the group cemented with resin-based temporary cement showed statistically significantly higher mean shear bond strength than non-eugenol temporary cement (P-value = 0.048).ConclusionBoth cleaning methods (mechanical and chemo-mechanical) applied in this study were effective in cleaning temporary cement remnants from the dentin substrate surface with statistically significant differences between results of shear bond strength with significantly higher values recorded with resin-based temporary cement.

In-vitro comparison of bonding time and strength of adhesive pre-coated and standard metal orthodontic brackets

To compare the shear bond strength and bond time of 3M Unitek's APC (Adehesive Pre-Coated) Flash-Free™system applied to metal brackets. An in vitro study was performed on 40 extracted sound human premolar teeth randomly divided into two groups (20 per group) bonded either with Adhesive Pre-Coated Flash-Free metal brackets or metal brackets coated manually with Transbond XT™ light-cure adhesive. Bonding time was measured using a stopwatch. Thermoycling was performed on the samples (500 cycles) to simulate the oral environment between baths of 5°C and 55°C distilled water. Debonding shear bond strength measurements were performed in an Instron universal testing machine. The APC Flash-Free group bonded in significantly (p<0.001) less time (mean 34.06s/tooth) than the manually coated group (mean 55.14s/tooth). Shear bond strength of the manually coated group was significantly (p<0.001) higher (mean 13.32 MPa) than the APC Flash-Free group (mean 10.95 MPa). The APC Flash-Free free system is efficient and allows for reduced chair time during the bonding appointment while attaining a mean shear bond strength of 10.95MPa, which is higher than the minimum shear bond strength of between 4MPa and 7MPa1

Metal-Seramik Diş Restorasyonlarının Üretiminde Farklı Yüzey İşlemlerinin Makaslama Bağlanma Dayanımına Etkilerinin Araştırılması

Aim: The bond strength between metal and porcelain is an essential factor for the success of metal-ceramic restorations. Therefore, this study evaluated the shear bond strength (SBS) between ceramic and cobalt-chromium (Co-Cr) alloys after oxidation treatment.
 Material and Methods: A total of 150 Co-Cr samples, 50 samples each, were produced from casting, laser sintering, and milling techniques. The primary group samples produced were divided into five subgroups. One of the subgroups is sandblasted with 110 µm Al2O3, and the others are ground with carbon separator disc, sintered diamond bur, tungsten carbide bur, and pink stone in one direction. SBS test was applied after the oxidation and veneering process. After debonding, digital microscopy investigated the surface characterizations of Co-Cr alloys. For the normality distribution of SBS measurements, the Kolmogorov-Smirnov test was used. According to the results, non-parametric tests were used in the study because the distribution was not suitable for the normal distribution, and the number of samples within the group was low in the subgroups. Kruskal Wallis and All pair-wise post hoc test (α = 0.05) were used for analysis.
 Results: There was a statistical difference between the laser sintering and milling groups according to the fabrication techniques. The highest SBS value was found in the Al2O3 laser group (34.35) and the lowest in the Al2O3 casting group (17.68). Surface treatments significantly altered ceramic adhesion. Almost all subgroups exhibited mixed failure. All of the SBS values found in this study were almost clinically acceptable.
 Conclusion: As different abrasives in the leveling and finishing of metal substructures may affect the metal-ceramic bonding, care should be taken in their use as much as possible.

Influence of Surface Conditioning on Bonding Polyetherketoneketone to Dental Ceramic

This study researched the effects of different surface conditioning techniques on the bond strength of polyetherketoneketone (PEKK) with lithium disilicate glass-ceramic material. Total of 105 test specimens were prepared from PEKK discs and randomly distributed into 5 experimental groups (n = 21) to which different surface conditioning techniques were applied. [Group A: sandblasting + SR Connect adhesive agent (SRC), Group B: dichloromethane (DCM) + SRC, Group C: methyl methacrylate (MMA) and DCM mixture + SRC, Group D: sandblasting + DCM + SRC, Group E (control): sandblasting + Pekk Bond adhesive agent (PB).] Surface roughness values of PEKK test specimens were measured. They were bonded to lithium disilicate glass-ceramic test specimens with resin cement. Half of them were subjected to thermomechanical aging. Shear bond strength measurements were made. Among the A, B, C, D, and E groups, a statistically significant difference was observed in terms of the surface roughness values (p < 0.001). Statistically significant differences were obtained among the thermomechanical aging groups (p < 0.001) and among the non-thermomechanical aging groups (p = 0.012) in terms of shear bond strength. Group D and Group E demonstrated clinically acceptable bond strength values when bonding PEKK material with lithium disilicate glass-ceramic material.

A remineralizing orthodontic etchant that utilizes calcium phosphate ion clusters.

This study aimed to investigate whether a phosphoric acid (H3PO4) solution containing calcium phosphate ion clusters (CPICs) could minimize enamel damage during long-term bracket bonding by dissolving the enamel surface and promoting enamel remineralization. The experimental design is as follows: first, three experimental etchants (H3PO4, CPICs-incorporated H3PO4 solution-I, and CPICs-incorporated H3PO4 solution-II) and two bonding resins (conventional orthodontic resin and self-adhesive orthodontic resin) were used in combination to create six groups, respectively. Each of these six groups was then divided into two sub-groups based on the presence or absence of thermocycling (TC). Twenty samples were assigned to each of the 12 groups (independent variables), and thus a total of 240 metal bracket-attached human premolars were used in this experiment. Bracket debonding was performed on each of 20 premolars in 12 groups, and shear bond strength (SBS) and adhesive remnant index (ARI) values were measured as dependent variables. Next, the three experimental etchants were applied (independent variables) to each of the three enamel samples, and the remineralization of the enamel surface was investigated as a dependent variable. The enamel surface was observed using electron scanning and atomic force microscopy. Furthermore, X-ray diffraction, energy dispersive spectroscopy (EDX) spectrum X-ray spectroscopy, and elemental mapping were performed, and the Knoop microhardness scale was measured. Therefore, the experiment was performed in two steps: SBS and ARI measurements for 12 groups, followed by observation of the enamel surface and microhardness measurements, according to the three types of etchants. As a result of the experiment, first, when the bracket was debonded, SBS did not decrease, and residual adhesive was hardly observed in the C2A group (before TC), C2A, and C1C groups (after TC) (p < 0.001). Second, the experimental etchant containing CPICs achieved remineralization while demineralizing the enamel. This was verified through SEM/EDX, element mapping, XRD, and AFM. Also, the roughness and microhardness of the enamel surface were better in the remineralized surface by the experimental etchant containing CPICs (p < 0.017). The CPICs-incorporated H3PO4 solution reduced ARI while maintaining SBS during bracket debonding, regardless of whether TC was performed or the type of resin. The etchant containing CPICs was also shown to remineralize the enamel and increase its microhardness.

Mechanical Properties of SDR™ and Biodentine™ as Dentin Replacement Materials: An In Vitro Study

The aim of this study is to evaluate the shear bond strength of nanohybrid composite resins (NCR) and microhybrid composite resins (MCR) placed over three different dentin replacement materials: SDR-Smart Dentin Replacement™, Biodentine™, and resin-modified glass ionomer cement (RMGIC). Thirty acrylic blocks (50 mm × 20 mm × 15 mm), each with a central hole, were prepared, which were randomly distributed into three equal groups, each corresponding to one of the three dentin replacement materials-SDR, Biodentine, and RMGIC. The central holes were then filled with these materials. After setting and application of the respective adhesive system, the specimens were further divided into two subgroups each of NCR or MCR. The respective composite material was then applied to the dentin replacement materials using a cylindrical plastic matrix. Shear bond strength was tested on a universal testing machine (Instron 3366), at a crosshead speed of 1.0 mm/minute. SDR attained consistently higher shear bond strength (means: 21.18, 22.19 Mpa) values than RMGIC and Biodentine, with both types of composite resins (MCR and NCR), which were statistically significant (p <0.001). When considering the means of the shear bond strength measurements obtained by the two types of the composite resin, no significant difference (p <0.05) was found between them with all three types of dentin replacement materials. There is no significant difference in the bond strengths achieved between MCR and NCR to the different dentine replacement materials. Hence, either type of composite resin may be expected to achieve similar bond strengths to the underlying substrate. SDR™ is a suitable dentine replacement material for placing below a composite resin veneer as it can achieve immediate higher bond strengths. SDR can be used as an effective bulk fill material in deep dentinal caries which can be capped with composite resins.

Application of neuro-fuzzy estimation in prediction of shear bond strength between concrete layers through the efficient laser roughness analyzer

To ensure the monolithic behavior of reinforced concrete composite parts, the bond strength at the interface between concrete layers cast at various ages must be high. Reinforced concrete composite members include precast beams with cast-in-place slabs, bridge decks strengthened by adding a new concrete layer, and repair and strengthening of existing concrete structural members by adding a new concrete layer. in this study, the shear bond strength (SBS) of reinforcing steel on Portland cement and a hybrid cement including slag and Portland cement activated with sodium carbonate is investigated. The pull-out test was used to determine SBS; also a subsequent test data is evaluated using ANFIS, as well as surface classification utilizing a laser roughness analyzer designed particularly to assess the roughness of the concrete substrate. As a result, this research tried to create an in situ non-destructive approach for assessment of concrete surfaces and its influence on shear bond strength measurement of the concrete layers. All test data is analyzed using an adaptive neural fuzzy inference system (ANFIS) to classify the different input variables for determining the shear bond strength between concrete layers using the mean and maximum surface roughness (SR) height parameters Ra and Rt in X and Y direction. ANFIS was used to optimize the process based on five processing parameters. Skillful prediction could play a pivotal role in the optimal conditions during laser cutting process. Based on results, laser speed is the most influential on the Ra in X and Y direction (RMSE: 0.3255, RMSE: 0.6869, respectively). The most influential parameter on the Rt in X direction is laser power (RMSE: 1.5611), while the most influential parameter on the Rt in Y direction is laser speed (RMSE: 2.0781), resulting that the roughness of the substrate surface highly affects the shear bond strength of concrete interfaces.

Effect of Airborne-Particle Abrasion Protocols and MDP-based Primer on the Bond Strength of Highly Translucent Zirconia.

To evaluate the effects of airborne-particle abrasion and MDP (methacryloyloxydecyl dihydrogen phosphate)-based primer treatment on the strength of resin bonds to highly translucent zirconia. Eight groups (n = 20 per group) of specimens were prepared with airborne-particle abrasion treatments (0.1-, 0.3-, or 0.6-MPa pressure) or not (untreated control) and MDP-based primer (treated) or not (untreated). Shear bond strength (SBS) tests were performed on the composite-to-ceramic bonded specimens either with or without thermocycling. After airborne-particle abrasion, the surface topography was evaluated by white light interferometry, and a phase analysis was conducted with x-ray diffraction (XRD). Surface roughness (Ra), surface energy (SE), and SBS measurements were statistically analyzed using either Tukey's HSD or the Kruskal-Wallis test, based on applicability. Lastly, the failure mode was observed by optical microscope and scanning electron microscope. Airborne-particle abrasion resulted in significantly larger Ra (p < 0.05), especially with higher treatment pressures. Treatment with MDP-based primer caused significantly higher SE and SBS than airborne-particle abrasion alone (p < 0.05), both with and without aging. MDP-based primer can enhance the bond strength and reduce hydrolytic aging of the bonded interface for highly translucent zirconia, exceeding the effects of airborne-particle abrasion. It is recommended that MDP-based primer treatment be applied with a composite cement containing adhesive phosphate monomer.

Cold Atmospheric Plasma Improves Shear Bond Strength of Veneering Composite to Zirconia.

Chipping of veneering is the most common clinical complication for zirconia restorations. Veneering composite could be a promising alternative to renew restorations. Zirconia discs (3-YSZ) were prepared with varying surface treatments and bonded to indirect composite as follows: air abrasion and Scotchbond Universal (A/SU); air abrasion and Clearfil Ceramic Primer (A/C); air abrasion and MKZ Primer (A/M); air abrasion and Monobond Plus (A/MP); silica-coating and Scotchbond Universal (S/SU); air abrasion (AP/SU), additional cold atmospheric plasma treatment, and Scotchbond Universal. An indirect composite material was then applied to the zirconia specimens. Specimens were divided into subgroups for short-term (14 days storage at 37 °C and 5000 thermal cycles) and long-term (250 days storage and 37,500 thermal cycles) artificial aging. Shear bond strength measurement (SBS) was performed, and data were analyzed by Kruskal–Wallis-test and multiple comparison testing with Dunn’s correction (p ≤ 0.05). The median SBS values (MPa) of short- and long-term artificial aging were: 3.09/1.36 (A/SU); 0.77/1.43 (S/SU); 2.82/2.15 (AP/SU); 1.97/1.80 (A/C); 2.01/1.58 (A/M); and 1.70/1.68 (A/MP). For short-term artificial aging A/SU showed the highest median SBS values, whereas in the long-term trial, AP/SU showed the highest values and the difference was significant. A prolonged artificial aging decreased SBS in all groups, except S/SU. In summary, treatment with CAP can improve SBS in the long-term.

Comparison between Mineral Trioxide Aggregate Mixed with Water and Water-based Gel Regarding Shear Bond Strength with Resin-modified Glass Ionomer Cement and Composite

To compare between mineral trioxide aggregate (MTA) mixed with water and water-based gel regarding shear bond strength with resin-modified glass ionomer cement (RMGIC) and composite. In this study, 40 blocks of cylindrical shape were prepared with acrylic. These blocks were divided into four groups with each group consisting of 10 blocks: group-1A: MTA + distilled water + composite, group-1B: MTA + distilled water + RMGIC, group-2A: MTA + polymer + composite, and group-2B: RMGIC + MTA + polymer. After that, a universal testing machine was used for the measurement of shear bond strength. The acrylic blocks were placed under this machine. A blade with a knife-edge was used to provide a crosshead speed of 1 mm/minute. This was continued till bond of MTA in both forms (distilled water/gel) and restorative material failed. It was observed that a statistically significant difference was found between MTAw + composite and MTAg + composite resin but no statistically significant difference between MTAw + RMGIC and MTAg + RMGIC with p ≥ 0.05. It was found that a statistically significant difference was present between the RMGIC and composite groups within the same MTA type with p ≤ 0.05. It was concluded from the present study that MTA with a water-based gel has a better shear bond strength than composite resin and RMGIC materials. It has been found that MTA has different properties when it is mixed with polymer and water. Very few studies have been conducted in the past to compare MTA mixed with water and water-based gel regarding the shear bond strength with RMGIC and composite.

Shear bond strength of veneering composite to high performance polymers.

High performance polymers like PEEK (polyetheretherketone) and FRC (fiberreinforced composite) could substitute metallic alloys for removable partial dentures. However, these polymers require aesthetic veneering. This study was to determine the bond strength to direct composite. Specimens made of PEEK and FRC were produced and air-abraded (50 μm aluminum-oxide). Specimens were allocated to four experimental groups: Luxatemp Glaze & Bond, Scotchbond Universal, SR Nexco Connect and iBond Universal. Specimens were divided into three subgroups for short-term, long-term and no artificial aging and shear bond strength (SBS) was evaluated. SBS of specimens made of PEEK with no artificial aging showed values between 10.79-14.00 MPa, short-term artificial aging resulted in values between 3.78-13.85 MPa and after long-term artificial aging SBS decreased to 0-8.75 MPa. SBS measurement of FRC specimens resulted in values between 9.83-12.1 MPa without aging, after short-term artificial aging values decreased to 8.36-11.98 MPa and after long-term aging SBS showed a degradation to 4.52-7.82 MPa.

Comparison of different standardised bond strength tests and the influence of glycine powder treatment in composite resin repairs

Aim: The repair of restorations is an eligible method to extend the survival rates of intraoral restorations. There is a consensus that the old surface has to be removed before repair by the use of a sandblaster or rotating instruments. This study aimed to investigate whether a glycine powder can be used successfully in composite repair by measurement of shear and tensile bond strength according to dental standards.&#x0D; Methodology: The influence of mechanical preparation by no powder, 25 µm glycine powder or 50 µm aluminium-oxide powder and chemical conditioning by the use of bonding, phosphoric acid and bonding or bonding, phosphoric acid and a silane on the repair bond strength of an artificially aged nano-hybrid composite was tested according to the guidelines of DIN 13990 (2017), ISO 29022 (2013) and ISO/TS 11405 (2015). The fracture modes were evaluated by adhesive, cohesive or mixed failures.&#x0D; Results: There was no significant difference in the performance of the different mechanical and chemical treatments. The shear bond test according to DIN 13990 (2017) produces higher repair bond strengths (26.0±8.9 MPa) than the test described in ISO 29022 (17.9±6.3 MPa). The tensile bond strength according to ISO/TS 11405 (6.9±1.8 MPa) was the lowest. Most adhesive failures occurred with the shear test according to ISO 29022 (41%), followed by DIN 13990 (18%) and the tensile test (4%).&#x0D; Conclusion: For evaluating the bond strength of composites the test described in ISO 29022 is recommended, because it produces the highest percentage of adhesive failures. Nano-hybrid-composites are robust to different repair protocols.&#x0D; &#x0D; How to cite this article:&#x0D; Herrmann GP, Reimann S, Daratsianos N, Weber A, Keilig L, Nadal J, Bourauel C. Comparison of different standardized bond strength tests and the influence of glycine powder treatment in composite resin repairs. Int Dent Res 2020;10(1):36-43. https://doi.org/10.5577/intdentres.2020.vol10.no2.2 &#x0D; &#x0D; Linguistic Revision: The English in this manuscript has been checked by at least two professional editors, both native speakers of English.

Management of caries affected dentin (CAD) with resin modified glass ionomer cement (RMGIC) in the presence of different caries disinfectants and photosensitizers.

To evaluate Shear bond strength (SBS) of resin modified glass ionomer cement (RMGIC) on caries affected dentin after using different cavity disinfectants i.e., chlorhexidine gluconate (CHX), Er,Cr:YSGG laser (ECYL) and photodynamic therapy (PDT). Total 50 freshly extracted mandibular molars were obtained through non-traumatic extraction. All the samples were rooted vertically within self-cure acrylic resin blocks up to cervical level so that only coronal portion remain visible. Silicon carbide grinding discs 1200 and 600 grits was used to prepare the teeth. However affected dentin remains untouched. All samples were randomly distributed in to five groups (n = 10). Group 1: 2 % CHX, Group 2: 2 % solution of methylene blue (MB) and Diode laser, Group 3: Indocyanine green (ICGP) solution and Diode laser, Group 4: curcumin (CP) and LED curing unit, Group 5: ECYL. The specimens were then stored at a temperature of 37 °C for 24 h and 100 % humidity before specimens were placed in to universal testing machine for the SBS measurements. Failure mode examination was performed by a stereomicroscope. ANOVA test analyze inter group comparison. Tukey HSD test was used to analyze multiple group comparison. The level of significance was set at p < 0.05 value. Among all the groups, group 1 (control, CHX treated) demonstrated highest SBS value (18.31 ± 1.06 MPa). Whereas lowest SBS was displayed by group 2 (PDT, MB) (12.31 ± 0.57 MPa). Dentin disinfected with group 4 (PDT, CP) (16.86 ± 0.97 MPa) and group 5 (ECYL) (17.39 ± 2.26) showed comparable result to that of CHX (p > 0.05). Bond strength of RMGIC bonded to CHX disinfected caries affected dentin was highest among study groups. Use of MB showed lowest shear bond strength outcomes. Moreover, application of ECYL and curcumin with LED showed bond strengths comparable to CHX control.

Effect of Er:YAG Laser Etching on the Shear Bond Strength and Microleakage of Self-Glazed Zirconia Ceramics.

Objective: To investigate the effect of Er:YAG laser irradiation on the shear bond strength (SBS) and microleakage of self-glazed zirconia (SZ) ceramics. Background: SZ is a novel type ceramic; laser irradiation has started to be used in the surface treatment of different ceramics, while SZ has been rarely studied to improve the bond quality. Methods: One hundred twenty blocks (5 mm × 5 mm × 5 mm) of SZ ceramics were produced and split into eight groups following different surface treatments (n = 15): Group A: no treatment; Group B: standard grid processing; and Group C-H: different Er:YAG laser power settings (100, 200, 300, 400, 500, and 600 mJ). Ten blocks of each group received the measurement of SBS and fracture mode analysis, three blocks underwent the evaluation of the microleakage depths, and the other two blocks were observed under the scanning electronic microscopy (SEM). Results: Group F obtained the highest SBS and the lowest microleakage depth without damaging the ceramic surface structure, which was statistically significant compared with the control group and gridding group (p < 0.05), whereas the difference was not statistically significant (p > 0.05) between group E and group F. The results of bonding performance were consistent with failure types and observation of surface characterizations in SEM images. Conclusions: According to the results here, Er:YAG irradiation had effect on surface treatment. In addition, 400 mJ Er:YAG could increase the SBS and decrease the microleakage depth on SZ ceramics without damaging the surface structure.

The Effects of Aluminablasting on Bond Durability Between Universal Adhesives and Tooth Substrate.

The aim of this study was to determine the effect of aluminablasting on the bond durability of universal adhesives and adherent surface characteristics. Adhese Universal (Ivoclar Vivadent), All-Bond Universal (Bisco), Bondmer Lightless (Tokuyama Dental), G-Premio Bond (GC), and Scotchbond Universal (3M ESPE) were used in self-etch mode. The prepared bovine enamel and dentin specimens were divided into two groups based on whether they received an aluminablasting prior to application of the universal adhesives. The resin composite bonded specimens were stored in distilled water at 37°C for 24 hours, following which the shear bond strength (SBS) of half of the specimens was measured (24-hour group). The other half was subjected to 30,000 thermal cycles between 5 and 55°C before SBS measurement (TC group). Surface roughness (Ra) and surface free energy (SFE) of the adherent surfaces were also measured, and scanning electron microscopy observation and scanning electron microscopy/energy-dispersive X-ray analysis were carried out. Most of the adhesives did not show any significant differences in enamel SBS values between the two pretreatment groups, regardless of the storage condition. However, the dentin SBS values were significantly lower in specimens that underwent aluminablasting compared with those that did not, irrespective of their storage conditions. Significantly higher Ra and SFE values were observed in the enamel and dentin of specimens that underwent aluminablasting. Although aluminablasting increased the Ra and SFE values of enamel and dentin, its effect on the SBS value was dependent on the tooth substrate. In addition to C, O, Na, Mg, P, and Ca, the element Al was detected in the enamel and dentin of samples that had undergone aluminablasting. These results suggest that although aluminablasting of the tooth surface is thought to be effective for modification of the adherent surface, it may not enhance enamel bond performance and may also adversely affect the dentin bond effectiveness of the universal adhesives.