Optically Stimulated Luminescence Measurements Research Articles

Light-induced fading effects on TL and OSL signals and feasibility of dose re-assessment with PTTL signals in BeO dosimeters

Abstract This study aims to investigate both light-induced fading effects on thermoluminescence (TL) and optically stimulated luminescence (OSL) signals under three different light sources (fluorescent, UV-254 and daylight) and dose reassessment with phototransferred TL (PTTL) signals in Beryllium oxide dosimeters. TL and OSL signals were deconvoluted for each light source. Accordingly, variations in the maximum peak temperature, activation energy, peak area value for the TL signal, and intensity and lifetime values for the OSL signal were monitored. Each peak, OSL component, and total area value exhibited different behaviors depending on the light source. Considering the total area condition, the TL intensity decreased by ∼90%, ∼80%, and ∼70% in UV-254, daylight, and fluorescent light exposure, respectively, at the end of the 120 min. On the other hand, the OSL total area intensity faded quickly for both UV-254 and daylight, while it decreased by ∼45% for fluorescent light. According to these results, regardless of TL and OSL measurements, the dosimeters should be kept primarily away from daylight and fluorescent light after irradiation, instead of UV-254, which is rarely encountered in daily life. The feasibility of dose reassessment using PTTL signals under UV-254 light was investigated within a wide dose range from 0.1 to 128 Gy. It is feasible to reassess doses between 0.5 and 32 Gy considering the total area intensity of PTTL signals. In conclusion, PTTL signals can be easily used in fields of the order of Gy, such as in reevaluating doses in radiotherapy applications.

Correlations between quartz OSL dose-response curve and TL glow curve characteristics, and their implications for equivalent dose estimation

Optically stimulated luminescence (OSL) dating of quartz using the single-aliquot regenerative-dose (SAR) procedure requires construction of dose-response curves (DRCs). The shapes of DRCs and their characteristic saturation doses (D0 values) are well-known to be highly variable between samples and among individual grains from the same sample, but the factors that control DRC characteristics are imperfectly understood. Here we report correlations between OSL DRC shapes and thermoluminescence (TL) glow curve characteristics for a sample of quartz from northern Australia. Individual grains were measured using the SAR procedure and one of two preheat temperatures (160 °C and 260 °C), and grouped according to similarities in their DRC shapes. Grains from each DRC group were then physically transferred onto a separate disc for TL measurement as a multi-grain aliquot. A strong correlation was observed between DRC group and laboratory-irradiated TL glow curve shapes, along with some differences between the two preheats. Irrespective of the selected preheat, earlier saturating DRC groups are associated with the most intense 110 °C TL signal, and the least intense 325 °C TL signal, which corresponds to the main OSL trap. Later saturating DRC groups generally show the opposite trend. There are also trends within other regions of the glow curve and DRC group, such as prominent TL responses at 140–160 °C, 220–240 °C and 390–410 °C. We assessed the effect on the accuracy of equivalent dose (De) estimation using an associated radiocarbon age as an independent cross-check of the OSL ages for the DRC groups. De over- and under-estimates were obtained for some DRC groups. Most notably, grains preheated to 160 °C displayed a pattern of De values which decreased with an increase in D0. We relate this to variable concentrations of charge at the ∼230 °C TL trap prior to regenerative dose OSL measurements. OSL ages for most DRC groups preheated to 260 °C are close to the radiocarbon age, as are those of later saturating DRC groups preheated to 160 °C; the latter DRC groups have the smallest TL signals at ∼230 °C relative to the TL peak at 325 °C. The results of this study suggest that correlations between single-grain De and D0 values can occur due to underlying differences in the TL characteristics of grains with different DRC shapes. In the absence of independent age control and prior to measuring multi-grain aliquots of quartz, we recommend that OSL dating practitioners screen their samples for any single-grain patterns of De as a function of DRC shape, to determine the optimal SAR measurement conditions and data-analysis procedures for De estimation.

Optically stimulated luminescence of Durolon polycarbonate

This paper reports for the first time the study of optically stimulated luminescence (OSL) of amorphous Brazilian bisphenol-A polycarbonate (Durolon) exposed to beta radiation. The OSL was studied from two perspectives: characterizing the luminescent signal as a function of radiation dose and examining repeatability. Computational analyses are applied to OSL curves via the deconvolution method. Fluorescence measurements employing the emission - excitation matrix (EEM) technique and optical absorption (OA) are incorporated to characterize the polymer defects and color centers. OSL measurements were carried out in a commercial reader Risø (model DA-20) coupled with a90Sr/90Y beta source. The sample was illuminated using 470 nm blue LEDs. The OSL response exhibited an exponential decay signal after 1 Gy, with linear dose-response and consistent repeatability. The continuous-wave-OSL curve was well adjusted with two distinct components. As result, Durolon promising potential as a luminescent dosimeter, supported by its desirable OSL signal characteristics.

A model explaining the optical bleaching of thermoluminescence in KMgF3:Tm fluoroperovskite

The aim of this work was to investigate the optical bleaching of the thermoluminescence of KMgF3:Tm fluoroperovskite. Thermoluminescence (TL) glow curves after optically stimulated luminescence (OSL) experiments were recorded. It was observed that only some of the traps responsible for the TL signal are depleted after the OSL measurements. Furthermore, these traps are not completely emptied even after long illumination times. A model is proposed that explains both the OSL and TL phenomena, as well as the optical bleaching of the TL signal after optical stimulation. Simulations were performed to support the proposed model.

Lateglacial and early Holocene evolution of the Tyne Valley in response to climatic shifts and possible paraglacial landscape legacies

This paper presents new sedimentological, geomorphological, and optically stimulated luminescence (OSL) geochronological evidence for fluvial evolution of the mid- to lower River Tyne through the Lateglacial to late Holocene. These data reveal a series of fluvial terraces produced by cycles of aggradation and incision, conditioned by glacial inheritance and driven by changing sediment availability and hydrological regime. The distribution and stratigraphy (where available) of nine river terrace and their associated sediments have been recorded. At two key sites the sediments have been dated using OSL measurements to constrain the fluvial geomorphology. Significant entrenchment of the fluvial system, followed by aggradation formed the earliest fluvial terrace (T1), which encompasses environments spanning the transition from deglaciation into Greenland Interstadial 1 (GI-1). Incision below T1 began towards the end of GI-1, with three terraces (T2 – T4) between the abandonment of T1 and the early Holocene (15.0–9.2 ka). Climatic shifts, limited vegetation cover/soil development, and peri−/paraglacial landscape instability conditioned the development of the early postglacial fluvial landsystem. Three further terraces (T5 – T7) developed during the mid- to Late Holocene (6.6–3.1 ka), and comprise most of the valley floor. Climatic instability, glacial inheritance, and widespread anthropogenic disturbances are reflected in greater hillslope-channel coupling during this period. The extent of later Holocene terraces (T8 – T9) is limited as the river became isolated from flanking hillslopes entrenched between existing river terraces. Fluvial landscape evolution in formerly glaciated catchments is strongly conditioned by the cold stage legacy that introduced excess sediment and landscape instability into the catchment. Subsequent catchment-wide responses are variable and non-linear, with valley floors operating in a series of reach-wide responses. There is a need for greater chronological control to constrain the Lateglacial and Holocene evolution in the Tyne catchment, but also to further our understanding of region-wide responses to external drivers and local dynamics.

Surface mount multilayer ceramic capacitors as optically stimulated luminescent dosimeters

The choice of dosimetric materials for precise retrospective dose assessment in case of any emergencies is very challenging. Since few decades, electronic components like ceramic resistors, inductors, IC chips, surface mount resistors and inductors have been proven to be suitable candidates for dose estimation using thermoluminesce (TL)/optically stimulated luminescence (OSL) techniques. In this work, OSL technique is applied to study dosimetric properties of surface mount multilayer ceramic capacitors (SM MLCC) available in commonly used instruments like printer, computer mouse, USB flash drive and personal gadgets like mobile phone etc. To understand the OSL process involved, the elemental composition and crystallinity of the SM MLCCs were analyzed using Fourier transform infrared (FTIR) and X-ray diffraction (XRD) techniques. It is found that the main constituent is barium titanate with aluminium silicate as major impurity along with some trace elements and is responsible for the origin of the radiation induced OSL signal. Some important dosimetric characteristics like OSL sensitivity, repeatability, OSL dose response, and OSL signal stability upon storage were studied. The stimulation time was optimized as 50 s and used for all OSL measurements. The dose response was found to be linear from 500 mGy to 15 Gy and simply increased (up to 40 Gy). Fading analysis showed that the OSL signal decreases by ∼ 25 % in 1 day, ∼ 50 % in 4 days, and remained stable after that at least up to 8 days. The dose was recovered using single aliquot regenerative-dose (SAR) technique with very good accuracy. These results of dosimetric studies and validation study suggest that surface mount multilayer ceramic capacitors have potential use as retrospective dosimeters.

Structural, mechanical, dielectric and defect properties of Eu-doped BeO ceramics: A computational and experimental approach

BeO ceramics in the wurtzite (w-BeO) form either pure or doped with lanthanide ions present high Thermoluminescence (TL) and Optically Stimulated Luminescence (OSL) sensitivity. However, the mechanism of defect formation governing the charge carrier dynamics associated with the TL and OSL signals is not well understood yet. Thus, this work aims to develop a study on the structural, mechanical, dielectric, and defect properties of Europium ion–doped w-BeO ceramics. We develop a new set of potential parameters to describe the Be–O bond. By using these potential parameters, we describe the physical and chemical properties with good agreement. Defect calculations employing the Mott and Littleton two-region strategy show that the distorted structure of pure w-BeO ceramics favours the Frenkel–type defect formation in the basal plane of the crystal lattice. When doped with Eu3+, we observed a change in the defect arrangement. It replaces preferentially two Be sites, eliminating beryllium interstices and keeping the beryllium vacancy from the initial configuration. We also observed that it is unlikely the Eu3+/Eu2+ coexist due to the solution energy values. Lastly, we have observed a most significant electron–hole interaction which may be associated with the intrinsic luminescence band of the w-BeO ceramics. In addition, TL and OSL measurements are presented to corroborate the defect calculations. The results presented here bring new insight to elucidate the charge carrier dynamic associated with the luminescent properties.

Further characterization of BeO detectors for applications in external and medical dosimetry

Measuring absorbed doses with high precision and accuracy for clinical applications using Optically Stimulated Luminescence (OSL) dosimeters can help to optimize treatment to patients. Beryllium Oxide (BeO) is a nearly tissue-equivalent material that has the potential to increase the applicability of OSL dosimetry in medical dosimetry, but there has been limited research into its characterization. We present here the characterization of BeO dosimeters in terms of annealing temperature and duration, the effect of preheat treatment on short-term fading, energy and angular dependence, and discuss possible errors in laboratory conditions by using the OSL technique. Shorter readoutof 30 s when using stimulation power of ∼30 mW cm2 is feasible but preheating then becomes necessary. The fading behavior of BeO was found to be dose-dependent in this case. Reproduciblity of an OSL measurement with repositioning of the dosimeter in the reader and for the short reaout times was found to be ∼1%. Energy response was close to the theoretical values, which agrees with some but differs from other published studies, indicating that the OSL efficiency might vary. The angular dependence presented the greatest uncertainty factor. In summary, BeO dosimeters have the potential to be used in clinical applications for dose evaluation. However, care should be taken while handling and applying an optimized measurement procedure is necessary due to the complex luminescence mechanism of the material.

Luminescence and ESR dating of the sedimentary infill from the multi-level cave system of Alkerdi-Zelaieta (Navarre, N Spain)

The finding of Upper Paleolithic engravings in 2016 triggered a multidisciplinary investigation of the Alkerdi cave system (Urdazubi, N Spain). The study of the speleogenetic processes led to the identification of at least 6 paragenetic cave levels with associated sedimentary infill. In order to unravel the timing of changes in the karst dynamics and to get some insights about sediment origin, two sediment samples were collected from cave levels 4 and 1 for numerical dating purpose, using both Optically Stimulated Luminescence (OSL) and Electron Spin Resonance (ESR) methods. One additional modern-age sample was also taken from the entrance of the karst to evaluate the magnitude of the optical bleaching achieved by the quartz grains before entering the cave system. Last, one sample was collected from a flowstone for U-series dating, providing independent age control. OSL measurements were carried out using small quartz multi-grain (MG) and single-grain (SG) Single Aliquot Regenerative-dose (SAR) protocol. Initial Equivalent Dose (D e ) results show evidence of saturated OSL signal for the sample of the higher level (with ∼60% of saturated aliquots). Unlike SA data, SG analyses do not meet the usual quality criteria (e.g., relatively high recuperation ratios, only a few grains with useable signal), suggesting that corresponding dating results should be treated with caution. Hence, both MG and SG TT-OSL and MG ESR methods were subsequently employed, as the corresponding signals are known to have higher saturation levels than OSL ones. ESR analyses were based on the Multiple Centre (MC) approach using the standard multi-grain multi-aliquot additive (MAA) dose method, while TT-OSL measurements were performed following Demuro et al. (2020). The latter, however, did not return any useful results for both samples. MC ESR data show the usual D e pattern (D e (Al)>D e (Ti op. D)>D e (Ti–H)) indicating that among the three ESR signals analyzed, the Ti–H most likely provides the closest estimate to the true burial age. However, low measurement repeatability and goodness-of-of fit indicate that the reliability of the ESR results may be reasonably questioned. Results derived from this multi-technique dating approach provide the first chronological constraints for the sedimentary infill of the Alkerdi cave system. In particular, they suggest that sediment deposition in Cave Level 4 (ALK-OSL01) occurred around 130 ka, which is in good agreement with the minimum age constraint given by the speleothem (80.5 ± 9.0 ka). In comparison, the young age obtained for sample ALK-OSL02 (5.0 ± 0.9 ka) suggests recent Holocene formation of the lowest cave level 1. Finally, the MG De value obtained for the modern sample is close to zero (<1 Gy), indicating that the OSL signal is almost fully reset at a multi-grain level before entering the cave. Additionally, despite the large De overdispersion measured in this modern sample, the De values are one to two order of magnitude lower than those obtained with the same model in the other two samples. Therefore, the large OSL D e overdispersion (OD) values of up to 64% obtained for the two samples from Cave Level 4 and 1 are most likely related to re-sedimentation processes inside the cave system.

Alexandrite: investigation of a natural material for radiation dosimetry

In this work we performed experimental analyses of the dose-response curves of natural alexandrite, using thermoluminescence (TL) and optically stimulated luminescence (OSL). The natural alexandrite crystals from Bahia, Brazil, were pulverized and the optical absorption measurements were carried out in the range of 200 to 800 nm, comparing a non-irradiated sample with a 10 Gy beta irradiated one. OSL and TL measurements were performed using the Risø equipment (model DA-20) with irradiation doses from 1 to 5 Gy. Glow curve analysis was done using GlowFit software for TL, and R Studio software for OSL measurements. The irradiated sample (10 Gy) shows an absorption spectrum similar to the non-irradiated one, containing the same bands. The samples of natural alexandrite showed a linear dose-response for both OSL and TL measurements. From the TL and OSL analyses, it was possible to infer a correlation between the slow OSL component with the most intense TL peaks of alexandrite.

The complexity of luminescence dating of tidal sand body revealed by the discrepancy of paired quartz OSL ages

Optically stimulated luminescence (OSL) dating is becoming a useful technique to yield absolute age of organic-poor sandy deposits. The buried tidal sand body (BTSB) in the coastal zone of northern Jiangsu Province, China, has been suggested to have the same origin as the offshore radial sand ridge in the Yellow Sea. However, chronological constrain of the BSTB is still quite limited. In this study, OSL measurements were conducted using silt-sized multi-grain and coarse-grained single-grain quartz to constrain the depositional history of a 25.6 m core from the BTSB. A low luminescence sensitivity of quartz was observed, and only ∼1.04% of the grains passed the standard rejection criterion for single-grain measurement. Analysis of paired OSL ages from two grain-size fractions using different protocols showed that silt-sized quartz ages were underestimated of 0.14–1.35 ka in comparison to coarse-grained quartz in the depth interval of 5.8–22.4 m. We interpret such an age discrepancy as the effects of lateral infiltration of fine-grained sediment into the sand body due to dynamic feature of channel-ridge system on the shelf. As far as we know, it is the first time that such infiltration is demonstrated through OSL dating. Our OSL data indicated that there is a significant hiatus between the Late Pleistocene stiff clay layer (50–18 ka) and the Holocene sequence. Holocene deposits only occurred in the last 2 ka, with rapid accumulation of ∼17 m-thick sediments at ∼2–1 ka, a slower accumulation between ∼1 and 0.1 ka and rapid land emergence through an accretion of ∼4 m-thick sediment over the past ∼0.1 ka. This study highlights the complexity of OSL dating in highly dynamic sedimentary environments. Therefore, examining different grain size fractions and comparing different measurement protocols are highly deserved in carrying out OSL dating in such environments. • We compared multi-grain silt-sized quartz and single-grain coarse-grained quartz ages for a tidal sand body. • Silt-sized quartz underestimated ages due to ‘younger’ sediment infiltration into tidal sand body. • The buried tidal sand body in the northern Jiangsu Province of China was formed in the last 2 ka.

SOIL ORGANIC CARBON DATING OF PALEOSOILS OF ALLUVIAL FANS IN A BLOWN SAND AREA (NYÍRSÉG, HUNGARY)

ABSTRACTThe most widely used dating techniques in quaternary research are the radiocarbon (14C) and optically stimulated luminescence (OSL) dating methods. In some environments, the investigated sediments do not contain enough material for14C dating. In these cases,14C dating of bulk sediment may be used as a last resort. The major aim of the present study was to determine the reliability and limitations of the different fractions of the soil organic carbon (SOC)14C ages in the Nyírség blown-sand study area, in Hungary. Therefore, the low- and high-temperature combustions of SOC (LT-SOC and HT-SOC)14C age of fossil soils were compared with the charcoal ages from the same fossil soil layer, and their (LT-SOC, HT-SOC, and charcoal) age reliability was verified independently by applying OSL to the quartz fraction of the sediment samples. The14C data show variable agreement with OSL ages. Charcoal fragments were collected from some of the best material for14C dating and their ages are in agreement with the LT and HT-SOC14C ages and OSL data. The14C age LT-SOC gives a reliable, credible ages, which were confirmed by independent OSL measurements. If buried soils do not contain any other macroscopic remnants for14C dating, the LT-SOC14C ages can be used, in the case of the Nyírség study area. The LT-SOC, which is the younger fraction of the soil organic carbon, may be considered to represent the burial time of the fossil soil layer. The HT-SOC14C ages are sometimes unrealistically older than expected and cannot be considered to be reliable.

Theoretical and experimental estimation of the relative optically stimulated luminescence efficiency of an optical-fiber-based BaFBr:Eu detector for swift ions

ABSTRACT The reliability of dose assessment with radiation detectors is an important feature in various fields, such as radiotherapy, radiation protection, and high-energy physics. However, many detectors irradiated by high linear energy transfer (LET) radiations exhibit decreased efficiency called the quenching effect. This quenching effect depends not only on the particle LET but also strongly on the ion species and its microscopic pattern of energy deposition. Recently, a computational method for estimating the relative efficiency of luminescence detectors has been proposed following the analysis of microdosimetric specific energy distributions simulated using the particle and heavy ion transport code system (PHITS). This study applied the model to estimate the relative optically stimulated luminescence (OSL) efficiency of BaFBr:Eu detectors. Additionally, we measured the luminescence intensity of BaFBr:Eu detectors exposed to 4He, 12C, and 20Ne ions to verify the calculated data. The model reproduced the experimental data in the cases of adopting a microdosimetric target diameter of approximately 30–50 nm. The calculated relative efficiency exhibits ion-species dependence in addition to LET. This result shows that the microdosimetric calculation from specific energy is a successful method for accurately understanding the results of OSL measurements with BaFBr:Eu detectors irradiated by various particles.

Dose response features of quenched and reconstructed, TL and deconvolved OSL signals in BeO

Despite the fact that Beryllium oxide (BeO) has been suggested by several research groups as an alternative passive radiation detector and dosimetric material, various concerns about supralinear dose response features were raised for both thermoluminescence (TL) and optically stimulated luminescence (OSL) signals of this material. This paper presents a detailed dose response study on BeO, for two different experimental conditions, namely for (i) the TL signal following irradiation at room temperature (RT), 125 and 200 °C and (ii) the CW – OSL signal measured at three different measurement temperatures (RT, 100 and 220 °C), following two different preheating temperatures (Tpre = 100 and 220 °C). The selection of these temperatures is based on the TL glow curve structure for BeO. The analysis was performed using (a) the actual experimental luminescence signals which suffer thermal quenching, and (b) by using the reconstructed luminescence signals, after correcting for thermal quenching. Deconvolution was performed only for the OSL signals. Intense supralinearity features for both TL peaks and OSL components are reported. Reconstruction affects greatly the dose response features of all TL signals, enhancing supralinearity. The dose response linearity coefficient μ of the dominant OSL component C1 is found to be independent of the preheating temperature. This provides a strong argument for the fact that the charge associated with this component originates mainly from the trap responsible for the TL peak 3 in BeO with Tm beyond 300 °C. Based on our experimental results, the supralinearity features of BeO are attributed to competition for free electrons by electron traps. The results of the present study suggest that competition takes place during both the irradiation and heating stages of a dose response experiment in BeO. Finally, preheating at 220 °C and subsequent OSL measurement at 100 °C is highly recommended as the optimum configuration for BeO, not only for roughly linear dose response but also in order to minimize transfer effects.

Extending the range of optically stimulated luminescence dating using vein-quartz and quartzite sedimentary pebbles

The feasibility of applying optically stimulated luminescence (OSL) techniques to obtain estimates of the burial age of lithic clasts in the form of pebbles of quartzose lithology is investigated in this study. We applied OSL measurement procedures to vein-quartz and quartzite pebbles from contexts at five sites with fluvial and coastal beach contexts of depositional age ranging from 500 ka to the mid Holocene. As in previous OSL studies with lithics, measured depth-dose profiles were interpreted to identify regions associated with key stages in the burial history of the pebbles, including the extent of pre-burial optical resetting, primary burial and any subsequent secondary stages of exposure to sunlight. While some of the pebbles had not been fully optically reset before burial, none were in field saturation, as commonly encountered with larger lithic clasts such as cobbles. The relatively low concentrations of radionuclides within vein-quartz and quartzite pebbles simplified the assessment of the radiation dose rate. OSL age estimates consistent with independent dating evidence were obtained for the three sites sampled in the UK (Langford Quarry, Leet Hill Quarry, Swanscombe Skull Site and Barnfield Pit) and one of two sites tested in Portugal (Forte Cão), whereas evidence of secondary optical bleaching detected in pebbles from a second site (Vale de Atela) underestimated the independent age for primary burial. The oldest depositional age of the contexts tested was ~500 ka (Leet Hill Quarry), and for some of the pebbles tested there was the capacity to extend the potential dating range further as the age equivalence of the limiting value of D e was in excess of 1 Ma. The advantages of working with smaller, portable, clasts in the form of pebbles and with a lithology of higher transparency opens up a wide range of potential applications, whether the depositional processes are environmental or anthropogenic in origin or modification. • New approach to the dating of Quaternary sediments containing vein-quartz and quartzite pebbles. • OSL techniques applied to sliced pebble cores produce depth-dose profiles that are related to optical exposure history. • Successful comparison of OSL ages with independently dated MIS 12, MIS 11, MIS 5 and Holocene depositional contexts. • Low dose rates for vein-quartz and quartzite pebbles potentially enable further extension of the dating range.

OSL with chips from US credit cards

Chips from credit cards issued by the major US banks have been tested with optically stimulated luminescence (OSL) as potential materials for use in emergency radiation dosimetry. The following dosimetric properties have been studied: (1) OSL decay curves from both irradiated and unirradiated samples; (2) dose-response characteristics of the OSL and values of minimum detectable doses; (3) fading of the OSL signal with time after irradiation. No OSL was detected in unexposed samples while prominent signals were observed after irradiation. It was found that the shape of the OSL signals can be fitted by a combination of an exponentially decaying function and a power function. The dose-response relationship was linear in the range 0–7 Gy if the OSL signals were measured at the same effective time after irradiation and normalized to the response to a test dose. Dose recovery tests demonstrated that the doses can be reconstructed with an accuracy ±20% if the OSL measurements are conducted within 7 days after exposure and the corresponding OSL doses are corrected for fading.

The potential of portable luminescence readers in geomorphological investigations: a review

AbstractThe development of functional portable optically stimulated luminescence (OSL) readers over the last decade has provided practitioners with the capability to acquire luminescence signals from geological materials relatively rapidly, which allows for expedient preliminary chronostratigraphic insight when working with complex depositional systems of late Quaternary age. Typically, when using the portable OSL reader, infrared (IR) or blue post‐IR OSL signals are acquired from bulk unprocessed materials, in contrast to regular luminescence dating, which is usually based on measurements on pure quartz or feldspar mineral separates, or on select silt‐sized polymineralic portions. To demonstrate the utility of portable OSL measurements, this paper outlines the basic features of portable OSL readers and their constraints. Subsequently, case studies in which the instrument has been used to elucidate cryptostratigraphic variations in sedimentary sequences for geomorphological applications are reviewed. The studies can generally be grouped into three main categories. The first includes studies where the variation of portable OSL reader luminescence signal intensities with depth are plotted to generate profiles that contextualize sediment stratigraphy. In the second group, portable OSL reader luminescence signal intensities are used to interpret sediment processes that shed light on depositional histories. In the last category, luminescence signals from the portable OSL reader are calibrated to approximate numerical burial ages of depositional units. The paper concludes with a discussion of possible future directions. © 2020 John Wiley &amp; Sons, Ltd.

Spatiotemporal variations and implications of luminescence sensitivity of quartz grains on the Chinese Loess Plateau since the last interglaciation

AbstractAlthough luminescence sensitivity of quartz grains of desert sands has been used in discriminating provenance, it still remains unclear about its spatiotemporal variations and climatic implications. In this paper, the luminescence sensitivity of quartz grains from the northern margin of the Chinese Loess Plateau (CLP) was studied using single-aliquot optically stimulated luminescence (OSL) and “pseudo” single-grain OSL measurements. Our results indicate that the OSL sensitivities have lower values in sand/loess beds and higher values in paleosols. We suggest that the variations in OSL sensitivity of quartz grains with depth on the CLP are mainly influenced by the origin of the quartz grains as they are related to the loess-sized material production processes and the migration of desert regions. More quartz grains of glacial origin with lower luminescence sensitivity, together with the reduced durations of irradiation and exposure cycles induced by shorter transport distance due to desert expansion, account for the lower luminescence sensitivity of glacial periods. Moreover, both the mountain processes and the retreat–advance of deserts are ultimately related to climatic changes, therefore, the orbital scale variations of luminescence sensitivity are controlled by glacial–interglacial oscillations on the CLP.

The evolution of the terrestrial‐terminating Irish Sea glacier during the last glaciation

ABSTRACTHere we reconstruct the last advance to maximum limits and retreat of the Irish Sea Glacier (ISG), the only land‐terminating ice lobe of the western British Irish Ice Sheet. A series of reverse bedrock slopes rendered proglacial lakes endemic, forming time‐transgressive moraine‐ and bedrock‐dammed basins that evolved with ice marginal retreat. Combining, for the first time on glacial sediments, optically stimulated luminescence (OSL) bleaching profiles for cobbles with single grain and small aliquot OSL measurements on sands, has produced a coherent chronology from these heterogeneously bleached samples. This chronology constrains what is globally an early build‐up of ice during late Marine Isotope Stage 3 and Greenland Stadial (GS) 5, with ice margins reaching south Lancashire by 30 ± 1.2 ka, followed by a 120‐km advance at 28.3 ± 1.4 ka reaching its 26.5 ± 1.1 ka maximum extent during GS‐3. Early retreat during GS‐3 reflects piracy of ice sources shared with the Irish‐Sea Ice Stream (ISIS), starving the ISG. With ISG retreat, an opportunistic readvance of Welsh ice during GS‐2 rode over the ISG moraines occupying the space vacated, with ice margins oscillating within a substantial glacial over‐deepening. Our geomorphological chronosequence shows a glacial system forced by climate but mediated by piracy of ice sources shared with the ISIS, changing flow regimes and fronting environments.

Quartz optically stimulated luminescence dating of loess in Tajikistan and its paleoclimatic implications for arid Central Asia since the Lateglacial

Thick and widespread loess deposits in southern Tajikistan provide insight into the regional climatic changes in arid Central Asia (ACA) during the Quaternary. However, because of the lack of robust chronological constraints, the environmental implications of these deposits are not yet fully understood. Here, we report a detailed medium-grained quartz optically stimulated luminescence (OSL) dating analysis on a loess sequence deposited since the Lateglacial in southern Tajikistan. The single-aliquot regeneration (SAR) and standardized growth curve (SGC) methods were used for equivalent dose determination. Quartz OSL measurements showed that both the SAR and SGC methods can be used for equivalent dose determination for Tajik loess. On the basis of the obtained OSL ages, we reconstructed the dust accumulation rates and mass accumulation rates. Our results show that the dust flux continued to decline whereas the precipitation increased stepwise after the end of the Last Glacial Maximum. Changes in the dust flux and precipitation in ACA were sensitive to the gradual warming since the Lateglacial.