High Temperature Corrosion Tests Research Articles

Ceramic matrix composites for corrosion-resistant next-generation nuclear reactor systems: A conceptual review of enhancements in durability against molten salt attack

Ceramic matrix composites (CMCs) are emerging as a key material class for enhancing corrosion resistance in next-generation nuclear reactor systems, particularly in high-temperature molten salt environments. These environments, critical for advanced nuclear reactors such as molten salt reactors (MSRs), present severe challenges, including aggressive chemical attacks that degrade traditional structural materials over time. This conceptual review explores the development and application of CMCs to improve the durability and corrosion resistance of nuclear reactors exposed to molten salt attacks. CMCs, which consist of ceramic fibers embedded in a ceramic matrix, offer significant advantages, such as high thermal stability, mechanical strength, and improved corrosion resistance compared to conventional materials. This review examines how CMCs can be tailored to withstand harsh operational conditions, with a focus on the selection of ceramic phases, fiber-matrix interactions, and innovative fabrication techniques that enhance their protective capabilities. Key challenges addressed include the optimization of composite design to resist molten salt corrosion, the effects of temperature on the material properties, and the long-term stability of CMCs under extreme conditions. Advances in surface treatments, coatings, and the development of hybrid CMC systems are also discussed, highlighting their potential to further enhance durability. The review outlines the use of advanced characterization techniques, such as high-temperature corrosion testing and in situ microscopy, to evaluate CMC performance in molten salt environments. Additionally, it identifies knowledge gaps in current research, emphasizing the need for long-term studies on CMC behavior under realistic reactor conditions. This review concludes by proposing future research directions and technological advancements required to integrate CMCs into next-generation nuclear reactor designs, aiming to improve system reliability and operational safety.

Improving hot corrosion behaviour of Cr3C2-25NiCr coatings by reinforcing nano yttria stabilized zirconia at 850 °C

Yttria-Stabilized Zirconia (YSZ)-enhanced Cr3C2-25NiCr coatings were applied to T22 boiler tube steel using the High Velocity Oxy Fuel (HVOF) method. Conventional Ni-20Cr, 5 wt.% YSZ- Cr3C2-25NiCr, and 10 wt.% YSZ- Cr3C2-25NiCr composite coatings were prepared. High-temperature corrosion tests were conducted on both uncoated and coated samples in a Na2SO4-60%V2O5 environment at 850°C under fluctuating thermal conditions. These experiments were carried out in a silicon tube furnace at high temperatures, with each sample subjected to 50 cycles of exposure. Each cycle consisted of 1 hour in the corrosive environment followed by 20 minutes of cooling at room temperature. Corrosion products were analyzed using energy-dispersive x-ray analysis (EDS) and scanning electron microscopy (SEM). The addition of YSZ to the Cr3C2-25NiCr coatings significantly improved corrosion resistance, with the Ni-20Cr, 5 wt.% YSZ-Ni-20Cr, and 10 wt.% Cr3C2-25NiCr coatings reducing overall weight gain by 73.08%, 84.70%, and 89.96%, respectively, compared to uncoated T22 steel.

Optimization of defects and high temperature corrosion resistance of laser cladding FeCrAl coatings: Influence of process parameters

To enhance the surface quality and high-temperature corrosion resistance of FeCrAl coatings further, a laser cladding technique was employed to deposit Fe-13Cr-7Al coatings on the surface of 12Cr1MoV heat-resistant steel. The study investigated the influence of laser power, scanning speed, and powder feed rate on the quality and high-temperature corrosion resistance of the Fe-13Cr-7Al coatings. Utilizing 25 orthogonal experiments, coatings were prepared and evaluated through high-temperature corrosion tests to explore the corrosion resistance and mechanisms microstructural analysis of the coatings, including their elemental distribution and corrosion mechanisms, was conducted using optical microscopy (OM), X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The optimal parameter combinations for laser cladding coatings were discussed. The results indicated that the coating quality was optimal within specific ranges of parameters (laser power 1875–2250 W, scanning speed 33–44 mm/s, powder feed rate 12–18 g/min); deviations outside these ranges led to issues such as incomplete coverage or coating detachment from the substrate. The structure of the laser cladded Fe-13Cr-7Al coatings consisted of columnar grains and α-Fe phase. In high-temperature corrosion testing, the coatings exhibited superior corrosion resistance compared to the substrate, with nearly twice the corrosion resistance variation observed under different process parameters. This study provides a scientific basis for optimizing laser cladding process parameters of Fe-13Cr-7Al coatings, demonstrating that precise control of process parameters significantly enhances the high-temperature corrosion resistance of coatings, thereby opening new possibilities for improving material performance in high-temperature applications.

High-temperature corrosion testing of titanium beryllides in the presence of water vapor and oxygen

Beryllium-based intermetallics are promising materials for the blankets of future fusion reactors and have potential applications in other areas of the nuclear industry, such as fission reactor reflectors and space technology. Understanding the high-temperature corrosion behavior of these materials in a noble gas medium containing chemically active impurities is essential for evaluating their suitability and guiding their application.This study investigates the high-temperature corrosion of titanium beryllide Be12Ti in the form of plate and grinded samples, produced by JSC “Ulba Metallurgical Plant” (Ust-Kamenogorsk, Kazakhstan). The corrosion tests were conducted under non-isothermal vapor-gas mixture (Ar + D2O or Ar + H2O flowing atmospheres) purging conditions using thermogravimetric (TG) analysis, differential scanning calorimetry (DSC), and mass-spectrometry of the gas phase.As a result of the corrosion tests, new experimental data on thermal effects have been obtained, describing the corrosion processes of Be12Ti samples across a wide range of temperatures and various heating rates in the presence of water vapor in the purge gas. The dependencies of sample mass change under heating conditions have been determined, and the characterization results of the samples before and after high-temperature corrosion tests are presented.Corrosion of titanium beryllides, both for Be12Ti plate and grinded samples, follows similar mechanisms. At around 500 °C, the mass of the samples begins to increase, and hydrogen isotopes are released. The test results indicate that corrosion of titanium beryllides with varying surface inhomogeneities proceeds similarly within the temperature range of 500–900 °C, showing a linear dependence on temperature.The results revealed significant insights into the oxidation mechanisms and the formation of corrosion products, which are crucial for optimizing the material's performance in fusion reactor environments.

Effect of Molten Salts Composition on the Corrosion Behavior of Additively Manufactured 316L Stainless Steel for Concentrating Solar Power

The effects of different molten salts on the corrosion resistance of laser powder bed fusion (L-PBF) 316L stainless steel was evaluated at 650 and 700 °C. The samples were characterized via XRD and SEM/EDX after high-temperature corrosion tests to evaluate the corrosion damage to the L-PBF 316L stainless steel caused by the molten salts. The presence of the salts accelerated the corrosion process, the chloride-based salts being the most aggressive ones, followed by the carbonate-based and the nitrate/nitrite-based salts, respectively. The L-PBF 316L did not react strongly with the nitrate/nitrite-based salts, but some corrosion products not found in the samples tested in the absence of salts, such as NaFeO2, were formed. LiFeO2 and LiCrO2 were identified as the main corrosion products in the samples exposed to the carbonate-based molten salts, due to the high activity of Li ions. Their growth produced the depletion of Fe and Cr elements and the formation of vacancies that acted as diffusion paths on the surface of the steel. In the samples exposed to chloride-based molten salts, the attacked area was much deeper, and the corrosion process followed an active oxidation mechanism in which a chlorine cycle is assumed to have been involved.

Experimental study of CO2/O2 corrosion on pipelines during carbon capture, utilization and storage process

In this paper, high-temperature and high-pressure corrosion test was used to simulate the corrosion process of multi-component thermal fluid (CO2/O2/H2O) on oil pipes (N80 steel), casings (J55, TP90H, P110 steel, and transportation pipelines (20# steel) in the process of CCUS technology application. The results show that during the entire corrosion process, the oil layer casing and surface casing are corroded most seriously in this environment, and the corrosion forms of these five steel materials in the CO2/O2 environment are uniform corrosion and local corrosion, and the corrosion products mainly consist of FeCO3, Fe2O3, Fe3O4 and FeOOH crystals. These oxides form a double-layer film structure on the surface of the steel. The inner layer is denser and consists mostly of FeCO3 crystals, which has better protection against further corrosion of the internal steel. The outer layer is loose and porous, and its components are mostly FeCO3 crystals. Fe2O3, FeOOH, Fe3O4 and FeCO3 crystals, have poor corrosion protection for internal steel. Due to the difference in corrosion products of the inner and outer film layers, relatively obvious local corrosion appeared on the surfaces of the 5 steel materials.

Corrosion Studies of Temperature-Resistant Zinc Alloy Sacrificial Anodes and Casing Pipe at Different Temperatures.

In order to solve the problem of external corrosion of deep well casing in oil and gas fields, a new type of high-temperature-resistant zinc alloy sacrificial anode material was used. The temperature and corrosion resistance of the new anode material and TP140 casing were investigated by simulating the high-temperature working conditions of a deep well in an oil field using high-temperature and high-pressure corrosion tests and electrochemical tests. The results showed that at 100-120 °C, the corrosion rate of TP140 protected by a sacrificial anode was only one-tenth of that under unprotected conditions, and the minimum corrosion rate of TP140 protected by a sacrificial anode at 100 °C was 0.0089 mm/a. The results of the dynamic potential polarization curve showed that the corresponding corrosion current density of TP140 first increased and then decreased with the increase in temperature. The self-corrosion potential in sacrificial anode materials first increased and then decreased with the increase in temperature, and the potential difference with TP140 gradually decreased.

The Influence of Protective Coatings on High-Temperature Corrosion under Biomass Ash Deposits

The presented research determined the performance of the protective coatings against the corrosion process under biomass and refuse-derived fuel (RDF) ash deposits. High-temperature corrosion tests were performed on steel grades intended for use in the fabrication of pressure parts working in elevated temperatures such as superheaters in power boilers. Two steel grades were investigated, P235GH and 16Mo3, and two protective coatings were applied, Inconel 625 and Alloy 310. The samples were sourced from the industrial boiler manufacturing company. The samples were exposed to two ashes originating from biofuels and one ash originating from RDF for comparison, all collected from Polish heat plants and power plants. Exposures were carried out in an oxidizing atmosphere for a maximum time of 504 h. The test temperatures of 480, 520, and 580 °C simulated superheater conditions of biofuel- and waste-fired power boilers. The corrosion kinetics were determined by weight change measurements conducted after 24, 168, and 504 h of the exposure. Regardless of the exposure temperature and the type of ash under which the samples were investigated, the use of 2.0 mm thick protective coatings resulted in smaller increases in the weight of the tested coupons which proves that alloy coatings give measurable results and are good remedies for chlorine-induced corrosion.

High-Temperature Corrosion Behavior of Selected HVOF-Sprayed Super-Alloy Based Coatings in Aggressive Environment at 800 °C.

This study is focused on the high-temperature corrosion evaluation of selected thermally sprayed coatings. NiCoCrAlYHfSi, NiCoCrAlY, NiCoCrAlTaReY, and CoCrAlYTaCSi coatings were sprayed on the base material 1.4923. This material is used as a cost-efficient construction material for components of power equipment. All evaluated coatings were sprayed using HP/HVOF (High-Pressure/High-Velocity Oxygen Fuel) technology. High-temperature corrosion testing was performed in a molten salt environment typical for coal-fired boilers. All coatings were exposed to the environment of 75% Na2SO4 and 25% NaCl at the temperature of 800 °C under cyclic conditions. Each cycle consisted of 1 h heating in a silicon carbide tube furnace followed by 20 min of cooling. The weight change measurement was performed after each cycle to establish the corrosion kinetics. Optical microscopy (OM), scanning electron microscopy (SEM), and elemental analysis (EDS) were used to analyze the corrosion mechanism. The CoCrAlYTaCSi coating showed the best corrosion resistance of all the evaluated coatings, followed by NiCoCrAlTaReY and NiCoCrAlY. All the evaluated coatings performed better in this environment than the reference P91 and H800 steels.

Study on high-temperature oxidation and hot corrosion characteristics of Cr60Ni40 laser cladding layer

In order to investigate the high-temperature characteristics of Cr-based alloy, Cr60Ni40 laser cladding layer (60 wt% Cr and 40 wt% Ni) were prepared and subjected to high-temperature oxidation test and hot corrosion test. The results prove that there are Cr segregation and large particles of Cr precipitated within the raw Cr60Ni40 cladding layer. During the high-temperature test, Cr2O3 protective film was generated on the surface of the cladding layer, protecting the substrate to different degrees. However, the particles precipitation of Cr caused uneven growth of Cr-rich oxide, and the Cr segregation brought about internal corrosion with Cr2O3 as the main products.

Comparison of Corrosion Behavior of T91, 9Cr and 9CrAl ODS Steels in Liquid Pb

It is important to improve the liquid lead corrosion resistance of fuel cladding alloy for promoting the development of lead-based reactors. The corrosion behaviors of traditional T91 steel and similar oxide dispersion strengthen ODS-type steels with or without the addition of Al, and were examined and compared at 600 °C in static oxygen-controlled liquid Pb in this research. High-temperature liquid lead corrosion tests were carried out for 120 h, 240 h, 500 h, 1000 h, and 2000 h, respectively, for three prepared samples. After the experiment, the corrosion behavior was evaluated and compared mainly based on the aspects of appearance, corrosion depth, microstructure, and composition difference. It was found that just the ODS design did not show a positive effect on corrosion resistance, while the addition of Al is beneficial to improving the corrosion resistance of ODS steel. The maximum corrosion depth of 9CrAl ODS is only 51.8 μm after corrosion for 2000 h, which is much lower than that of 9Cr-ODS steel. A thin film containing Al/Cr formed in the corrosion area after adding Al in 9Cr ODS steel, which played a positive role in corrosion resistance.

EXPERIMENTAL STUDIES ON HIGH-TEMPERATURE CORROSION INTERACTION OF TIN-LITHIUM ALLOY WITH STAINLESS STEEL AND REFRACTORY METALS

This article describes experimental investigations to determine the corrosion compatibility of candidate matrix materials of a capillary-porous structure (CPS) with a liquid tin-lithium alloy at high temperatures. The studies were conducted with the Sn75-Li25 alloy and samples of 12Ch18Ni10Ti grade austenite stainless steel, VEL-3 grade vanadium, and TT grade tantalum. Experiments on the interaction of a liquid tin-lithium alloy with candidate samples of the CPS matrix at high temperatures were carried out on an experimental TiGrA setup based on a TGA/DSC 3+ thermogravimetric analyzer. The paper provides a description of the methodology and conditions for conducting high-temperature corrosion tests. In the course of this work, experiments were carried out to study the compatibility of a tin-lithium alloy in the liquid phase with a stainless steel, vanadium and tantalum samples in the temperature range from 600 ℃ to 1000 ℃. Based on obtained results, the thermal effects of the processes occurring as a result of the interaction of the alloy with a candidate materials of the CPS matrix were determined. As a result of the analysis of the results obtained it has been revealed that at interaction of the studied materials with liquid tin-lithium alloy Sn75-Li25 at high temperatures complex physical and chemical processes take place, such as: selective dissolution of components by liquid alloy (solvent); penetration of component of liquid alloy (tin) into stainless steel depth; mass transfer of dissolved metals from solid metal into liquid.

Hot-Corrosion and Particle Erosion Resistance of Co-Based Brazed Alloy Coatings

Tape brazing constitutes a cost-effective alternative surface protection technology for complex-shaped surfaces. The study explores the characteristics of high-temperature brazed coatings using a cobalt-based powder deposited on a stainless-steel substrate in order to protect parts subjected to hot temperatures in a wear-exposed environment. Microstructural imaging corroborated with x-ray diffraction analysis showed a complex phased structure consisting of intermetallic Cr-Ni, C-Co-W Laves type, and chromium carbide phases. The surface properties of the coatings, targeting hot corrosion behavior, erosion, wear resistance, and microhardness, were evaluated. The high-temperature corrosion test was performed for 100 h at 750 °C in a salt mixture consisting of 25 wt.% NaCl + 75 wt.% Na2SO4. The degree of corrosion attack was closely connected with the exposure temperature, and the degradation of the material corresponding to the mechanisms of low-temperature hot corrosion. The erosion tests were carried out using alumina particles at a 90° impingement angle. The results, correlated with the microhardness measurements, have shown that Co-based coatings exhibited approximately 40% lower material loss compared to that of the steel substrate.

Investigating the Use of C/SiC Ceramic Composites in an Innovative Light-Water Reactor Core Grouping Catcher

China Nuclear Power Engineering, Northwestern Polytechnical University, and Beijing Institute of Technology have undertaken a joint research work with the goal of developing corium retention containers for use in an innovative light-water reactor core grouping catcher (CGC). In Serious Accidents (SAs), the corium will be retained in the C/SiC ceramic composite spherical shell container and thrown into the pool for passive cooling. In order to investigate the capability of the C/SiC ceramic composites to withstand the high temperature of 1800°C and the huge thermal shock at the initial stage of cooling, in this work, the high-temperature performance of these composites is studied. Furthermore, the compatibility of these composites with corium is investigated, and a retention container design prototype is proposed. The thermal conductivity, thermal expansion coefficient, high-temperature tensile strength, and thermal shock resistance of the candidate C/SiC specimens to be used in the manufacturing of the detention container are measured. The FactSage software package is used for the chemical compatibility study and product composition analysis of the composite SiC deposition layer and corium. The corrosion process of the SiC deposition layer of the composite material caused by corium is investigated through high-temperature corrosion tests and the electron microscopy analysis of the SiC specimen with the incorporation of CeO2. The results show that the C/SiC ceramic composite can meet the design criteria of the CGC corium retention container, and it is impossible to cause a carbon reaction disaster through the failure of the composite SiC deposition layer.

Synthesis and characterization of nano-SiO2@octadecylbisimidazoline quaternary ammonium salt used as acidizing corrosion inhibitor

AbstractAiming at the current situation that the existing acidizing corrosion inhibitors are difficult to apply in high temperature, high concentration acid, and other complex conditions, this article uses nano-SiO2as the core and preferably functional monomers to synthesize nano-SiO2@octadecylbisimidazoline quaternary ammonium salt (nano-SiO2@OBQA). Analytical methods such as nuclear magnetic resonance, infrared, and scanning electron microscopy were used for characterization. The corrosion inhibition performance of the N80 steel sheet by nano-SiO2@OBQA in 20% concentrated hydrochloric acid was studied using the high-temperature corrosion testing machine and adsorption isotherm model combined with quantum chemistry calculations to explore its mechanism of action. The results show that nano-SiO2@OBQA has good high-temperature resistance. When the temperature is 180℃ and the dosage of nano-SiO2@OBQA is 4%, the corrosion inhibition rate is 61.42 g·m−2·h−1. Studies have shown that the adsorption of nano-SiO2@OBQA on the surface of the N80 steel sheet follows the Langmuir isotherm adsorption model, which is spontaneous chemical adsorption.

Effect of Cr Content on Corrosion Resistance of Ni-xCr-Mo Laser-Cladding Coatings under H2S-Induced High-Temperature Corrosion Atmosphere.

Ni–xCr–Mo laser-cladding coatings with varying Cr content of 10, 15, 20, 25, and 30 wt.% were fabricated using a self-assembled coaxial laser-cladding device. The H2S-induced high-temperature corrosion tests under reductive atmosphere were conducted at 500, 550, and 600 °C. Subsequently, the influence of Cr content on the microstructural evolution and corrosion resistance of the Ni–xCr–Mo coatings was investigated. The experimental results revealed that 30 wt.% Cr is the limited maximum content that forms the suitable morphology of coatings without large prominent pores and cracks during the fabrication process, and 15 wt.% Cr corresponds to the critical minimum content for excellent corrosion resistance, as implied from the variation tendency of the corrosion weight-gain curves. Moreover, a two-layer structure of the corrosion scales was observed in the Ni–xCr–Mo laser-cladding coatings, which was primarily caused by the selective corrosion between the Ni and S and Cr/Mo and O.

High Temperature Chloride Corrosion Behavior of 904L:AlFeNiMoNb High-Entropy Alloy

In order to obtain high cost-effective coating materials working in chlorine-containing environment at high temperature, a 904L super austenitic alloy modified by an AlFeNiMoNb alloy (904L:AlFeNiMoNb) was obtained by vacuum arc melting process. The 904L:AlFeNiMoNb high-entropy alloy has a similar phase component with the AlFeNiMoNb alloy, but a more homogenous microstructure than that of the AlFeNiMoNb alloy. High-temperature chloride corrosion tests for 904L, AlFeNiMoNb, and 904L:AlFeNiMoNb high-entropy alloy were carried out under N2–2.6 vol.% CO2–1.3 vol.% O2–2,700 vppm HCl gaseous environment at 700°C and 800°C for 55 h, respectively. Due to the volatilization of FeCl2, weight change curves of the 904L alloy at 700°C and 800°C showed obvious weight loss. Especially at 800°C, the weight loss of the corroded 904L sample was 10 times that of the corroded sample at 700°C. Different from the weight loss situation of the 904L sample, both AlFeNiMoNb and 904L:AlFeNiMoNb high-entropy alloy showed small weight gains under the corrosion temperature of 700°C, while the latter gained half as much weight as the former. When the corrosion temperature was raised to 800°C, the AlFeNiMoNb and 904L:AlFeNiMoNb high-entropy alloy showed flat weight change curves with little weight loss. Weight loss for the AlFeNiMoNb and 904L:AlFeNiMoNb high-entropy alloy were 1.35138 and 0.0118 mg/cm2, respectively. The high temperature chloride corrosion resistance of 904L:AlFeNiMoNb high-entropy alloy is higher than that of 904L and AlFeNiMoNb at both 700°C and 800°C. Meanwhile, on the basis of the morphology and composition results of the corroded samples, combined with thermodynamic calculation, the high-temperature chloride corrosion mechanics of the tested alloys were discussed.

Degradation of engine components upon exposure to chemically modified vegetable oil - Based automotive lubricant

The present investigation examines the corrosion behavior of vegetable oil-based engine oil-biodiesel environment against automotive engine components, viz., cylinder liner, crankshaft, camshaft, journal bearing and timing gear as a counteractive measure. The biodegradable engine oil was formulated via chemical synthesis route and the thermo-oxidative stability of the biodegradable engine oil was analysed using thermogravimetric analysis. A high-temperature corrosion test rig was developed for the purpose of evaluating the corrosion behavior of biodegradable engine oil and the corrosion results were compared with those of synthetic engine oil SAE20W40 under similar test conditions. The corrosion penetration rate (CPR) of the journal bearing is 0.03270 ​mm/year and 0.0163 ​mm/year for biodegradable and synthetic engine oil respectively and the CPR of crankshaft, cylinder liner, camshaft and timing gear in biodegradable engine oil is 0.0120, 0.0156, 0.0127 and 0.0119 ​mm/year respectively, conversely in SAE20W40, the respective CPR is 0.0110, 0.0133, 0.0117 and 0.0109 ​mm/year. The scanning electron microscopy, X-ray diffraction, energy dispersive spectroscopy analysis of post corrosive surfaces revealed that biodegradable engine oil is prone to corrosion against various lubrication system components as compared to SAE20W40.

Comparison of high temperature corrosion resistance of NiCr-based coatings applied by High Velocity Oxygen Fuel and Twin Arc Spray processes

High temperature corrosion in a molten sodium sulfate salt environment is a serious problem of coal-fired boiler components. The promising possibility for surface protection is to apply thermally sprayed coatings. However, the key to success is to choose the optimal material and the proper spraying technology for a given application. Therefore, this study is aimed at a comparison of the high temperature behaviour of two protecting NiCr-based coatings sprayed by different technologies on 1.4903 (W.nr.) chrome-molybdenum steel. NiCrMoWFe was deposited by High Velocity Oxygen Fuel technology (HVOF). Twin wire arc spray technology (TWAS) was used to deposit multi-layered “multicoat” consisting of NiCrMoNbTa and NiCrTi with ceramic overlay Armaguard coated by brush. Chrome-molybdenum steel 1.7715 (W.nr.) commonly used in coal-fired boiler was also exposed to the high temperature corrosion test to evaluate the potential benefit of the coating. Coated as well as the uncoated specimens were exposed to the molten salt environment 18% Na2SO4 and 82% Fe2(SO4)3 at 690 °C under cyclic condition. The thermogravimetric approach was used to determine kinetics of corrosion. The X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS) techniques were used to analyze the corrosion products and determine the corrosion mechanism. The results of high temperature corrosion resistance show that NiCrMoWFe coated by HVOF and multicoat sprayed by TWAS was comparable.

High-temperature corrosion behavior of high-temperature and high-pressure cavitation processed Cr–Mo steel surface

In this paper, long-term high-temperature corrosion at 500 °C and high-temperature corrosion at the melting temperature of a corrosive ash mixture were examined because the use of high-temperature equipment such as boilers and gas turbines increases year over year. To investigate the optimum cavitation processing conditions for the specimens used in high-temperature corrosion tests, the surface properties of each processed specimen were examined. In specimens processed using multifunction cavitation (MFC), the compressive residual stress was high when the processing time was 10 min and the Cr content on the surface was greater than on the surface of an unprocessed specimen. On the other hands, in specimens subjected to water-jet peening (WJP), the compressive residual stress was high when the processing time was 10 min. In the present study, the processing time was selected to be 10 min and all high-temperature corrosion tests were conducted by the coating method. In the case of long-term high-temperature corrosion at 500 °C, the corrosion loss of the MFC-processed and WJP-processed specimens was small, whereas the corrosion loss of the unprocessed specimen was large.