Fiber Weight Fraction Research Articles

Effect of hygrothermal ageing on the mechanical properties of glass fiber reinforced polymer composite: Experimental and numerical approaches

This paper studied the effect of hygrothermal ageing on the mechanical performance of glass fiber-reinforced polymer composites (GFRPCs), a crucial material for marine applications due to its lightweight and superior resistance to environmental chemicals. However, prolonged exposure to moisture and temperature can degrade its properties, impacting structural integrity. The influence of moisture diffusion in GFRP composite laminates was evaluated by accelerated ageing tests, which involved submerging the composite laminate in seawater at 75°C until it reached full saturation. The composite laminates were fabricated with weight fractions of glass fiber reinforcements 55 %, 60 %, and 65 %. After two months of submersion, mechanical characteristics, namely tensile strength, modulus of elasticity, and interlaminar shear strength (ILSS) were investigated. A computational model was developed using COMSOL Multiphysics to analyse the coupled interfaces of moisture diffusion and heat. The failure mechanism of the GFRP composites was analysed using a scanning electron microscope (SEM). After two months of submersion, the moisture uptake data for the tension test samples showed a maximum saturation of 3.45 % for the 55 % fiber weight fraction, leading to a reduction in tensile strength from 269 MPa to 171 MPa and in modulus of elasticity from 24 GPa to 21 GPa. For the ILSS test samples, the maximum moisture saturation was 2.95 % for the 55 % fiber weight fraction, with a corresponding decrease in ILSS from 24 MPa to 21 MPa. However, increasing the glass fiber weight fraction from 55 % to 65 % resulted in improved tensile strength, modulus of elasticity, and ILSS in both as-manufactured and aged samples. The results of simulations and experiments showed that hygrothermal ageing causes the fiber surface to debond and causes matrix cracking, which in turn creates an uneven internal stress field.

Moisture-induced mechanical property changes in natural hybrid composites with mwcnt fillers

ABSTRACT This study investigates the moisture absorption behaviour and its effects on the mechanical properties of polyester composites reinforced with jute and hemp fibres. The differences in moisture absorption between distilled water and saltwater are examined. Tensile and flexural tests are conducted on pure jute fibre-reinforced polyester composite, pure hemp fibre-reinforced polyester composite, and jute (J-P) and hemp (H-P) fibre-reinforced polyester composite. Changes in mechanical properties due to varying moisture conditions are analysed. Furthermore, the impact of a synthetic nano filler, multiwall carbon nanotubes (MWCNTs), on these composites is assessed. The study reveals that MWCNTs enhance mechanical properties, particularly in moist conditions. Fracture behaviour analysis aids in understanding the interaction between natural fibres, the matrix, and nano-reinforcement. At maximum natural fibre weight fractions (40%), moisture absorption reaches 8.17% for the J-P composite in distilled water and 9.61% in saltwater, while the H-P composite shows maximum absorptions of 6.61% and 8.27%, respectively. The hybrid composite records 4.18% and 7.17% under similar conditions. Compared to the plain jute fibre-reinforced composite, the addition of multiwall carbon tubes into the polymer matrix significantly reduces the moisture absorption capacity of the jute composite to 34.89% and 31.30% for distilled water and saltwater, respectively.

Upcycling waste polypropylene with basalt fibre reinforcement enhancing additive manufacturing feedstock for advanced mechanical performance

This research seeks to overcome the printing and processing challenges of using waste polypropylene (PP) reinforced with short basalt fibres, transforming them into upcycled feedstock for additive manufacturing. It introduces an optimised method for producing filaments and 3D printing with these materials, addressing common issues such as adhesion and warpage through innovative techniques while achieving maximum mechanical performance in the resulting composites. Basalt fibre weight fractions of 0 %, 2 %, 5 %, 8 %, 15 %, 30 %, and 50 % were used to reinforce the recycled polypropylene, improving both printability and mechanical properties. The tensile strength reached 53.58 MPa at 15 % fibre content, while the flexural strength peaked at 34.06 MPa with 30 % fibre content, revealing distinct interactions between the fibres and polymer under tensile and flexural loading that were not previously observed. Microstructure, voids, debonding, and dispersion were examined using optical and scanning electron microscopy. Differential Scanning Calorimetry (DSC) was performed to assess the thermal behaviour and crystallinity of the recycled polymer during filament production and printing, revealing slight matrix degradation during these processes. The findings highlight the potential of waste basalt fibre-reinforced PP as a valuable filament feedstock for 3D printing, supporting a circular economy approach to composite manufacturing.

3D printing of high-stiffness and high-strength glass fiber reinforced PEEK composites by selective laser sintering

Glass fiber reinforced poly-ether-ether-ketone (PEEK) composites are emerging as structural materials of multifunctional devices in space applications, due to their outstanding mechanical properties, electrical insulating properties, and resistance to irradiation. Here, a new approach for preparing glass fiber/PEEK powders tailored for selective laser sintering (SLS) process is proposed. The surface of glass fiber is modified with the sulfonated PEEK following the designed procedure. The flowability of glass fiber/PEEK powders is also improved by adding the nano-scale SiO2 flow agent. The glass fiber reinforced PEEK composites are successfully 3D printed using the glass fiber/PEEK powders. Further, the enhancement of interfacial bonding between PEEK and glass fiber is analyzed through quasi-static tension tests and scanning electron microscopy (SEM) for the SLSed glass fiber reinforced PEEK composites. The average ultimate tensile strength reaches approximately 100 MPa using these optimal process parameters, while the average elastic modulus is around 7 GPa. Finally, the upper limit of fiber weight fraction is evaluated with the X-ray computed tomography (XCT) and the high-fidelity discrete element method (DEM) simulation.

Effect of Vibration Pretreatment-Microwave Curing Process Parameters on the Mechanical Performance of Resin-Based Composites.

The vibration pretreatment-microwave curing process can achieve high-quality molding under low-pressure conditions and is widely used in the curing of resin-based composites. This study investigated the effects of the vibration pretreatment process parameters on the void content and the fiber weight fraction of T700/TRE231; specifically, their influence on the interlaminar shear strength and impact strength of the composite. Initially, an orthogonal experimental design was employed with interlaminar shear strength as the optimization target, where vibration acceleration was determined as the primary factor and dwell time as the secondary factor. Concurrently, thermogravimetric analysis (TGA) was performed based on process parameters that corresponded to the extremum of interlaminar shear strength, revealing a 2.17% difference in fiber weight fraction among specimens with varying parameters, indicating a minimal effect of fiber weight fraction on mechanical properties. Optical digital microscope (ODM) analysis identified interlaminar large-size voids in specimens treated with vibration energy of 5 g and 15 g, while specimens subjected to a vibration energy of 10 g exhibited numerous small-sized voids within layers, suggesting that vibration acceleration influences void escape pathways. Finally, impact testing revealed the effect of the vibration pretreatment process parameters on the impact strength, implying a positive correlation between interlaminar shear strength and impact strength.

An in vitro wear behavior analysis of polymer composite for biomedical application.

The tribological performance of basalt fiber reinforced PEEK material especially used as a biomaterial in many biomedical and dental applications is of interest. The specimens of three different weight fractions of PEEK and basalt fiber are fabricated as per ASTM G99 standards. The prepared specimens are having PEEK and basalt fiber in the weight percentage of 90:10, 80:20 and 70:30 ratio and named as PBC 1, PBC 2 and PBC 3 respectively. The specimens are subjected to pin-on-disc test using EN31 steel as the sliding disc material. The hardness of PBC 2 specimen shows a better value of 50.74 HRB. Wear resistance is comparatively less when Basalt weight percentage increases from 10% to 20%, but further increase of basalt fiber in the composite, the wear resistance drops down. Similarly, the COF values also noted high for PBC 2 compared to pure PEEK, PBC 1 and PBC 3 composites. PBC 2 sample is found to be better with high wear resistance.

Enhancing wear resistance, mechanical properties of composite materials through sisal and glass fiber reinforcement with epoxy resin and graphite filler

This study investigates the mechanical and wears properties of sisal and glass fiber-reinforced epoxy composites with graphite as filler material. We assessed the mechanical properties of the hand-layup-fabricated composite materials, including hardness, tensile strength, flexural strength, and impact strength, by ASTM standards. We also performed wear evaluations using a pin-on-disc apparatus. The results showed that the weight fractions of sisal fiber, glass fiber, graphite, and epoxy resin significantly affected the mechanical properties of the composites. In contrast to composites reinforced with individual fibers, hybrid composites exhibited enhanced mechanical properties. The optimized compositions showed improvements in tensile, flexural, impact, and hardness properties. The wear analysis revealed that a variety of factors, including the weight percentage of reinforcement, sliding velocity, load, and sliding distance, had an impact on the composites' wear resistance. The SEM images provided significant insights into the composite material's micro structural characteristics and failure mechanisms. In general, this research showcases the potential of graphite filler-reinforced sisal and glass fiber epoxy composites for use in applications that demand exceptional abrasion resistance and mechanical strength. Further refinement of the composition and processing methodologies could lead to the development of composites tailored to specific application demands.

Characterization of Mechanical Properties of Coconut Coir Fibre Reinforced PLA Composites

This study examines the biodegradable and fracture toughness of Polylactic Acid (PLA) composites supplemented with coir fibres at different fibre weight fractions. Sustainable composite materials are made by combining fibres from coconut coir with PLA, a biodegradable polymer sourced from renewable resources. To improve their characteristics, the fibres are treated with sodium hydroxide, and twin-screw extrusion and injection moulding are used to create the composites. According to ASTM standards, tensile, impact, and flexural strength tests show that untreated coir fibre reinforced PLA composites have higher tensile and impact strengths than pure PLA, whereas treated fibres offer marginal increases at particular weight fractions.As fibre content rises, flexural strength often falls; untreated composites outperform treated ones in this regard. These results demonstrate the potential of PLA composites reinforced with coir fibre as greener substitutes for traditional polymers, with prospective uses in structural contexts where mechanical integrity and biodegradability are essential.

Testing and Evaluation of Hybrid Polymer Composites Reinforced with Moringa oleifera and Boehmeria nivea Fibers, Embedded with Copper Oxide Particulates, for Thermal, Structural, and Biological Properties

Abstract The increasing need for sustainable materials in industrial applications has prompted a significant shift in attention from synthetic to natural fibers. This study examines the problems and opportunities arising from the utilization of natural fiber-reinforced polymer composites in several industrial sectors. The objective of this work is to fabricate a hybrid composite using a conventional hand layup technique with natural reinforcement of Moringa oleifera (MO) and ramie (Boehmeria nivea) fibers, an epoxy matrix blended with copper oxide filler, utilized to enhance material stability and antimicrobial activity. To quantify the effect of five different weight fractions of MO and ramie fibers on this hybrid composite, its mechanical, thermal, functional, and antifungal properties were examined. The superior tensile strength (61.34 MPa), flexural strength (64.78 MPa), and impact energy (23 J) results indicate that ramie fiber loading should be increased. Additionally, enhanced thermal properties such as thermal conductivity (0.93 W/mK), heat deflection temperature (97°C), thermal expansion coefficient (1.7210−5/°C), and maximal thermal stability were observed at 347°C as a result of the increased ramie fiber loading. This analysis demonstrates that this hybrid composite possesses the antifungal activity necessary to form an inhibition zone against Candida albicans. Scanning electron microscopy analysis was conducted to determine the hybrid composites’ bonding strength and failure mode.

Tensile strength and stiffness properties of additively manufactured PET-G polymer-based composite plates reinforced with different weight fractions of short carbon fibers

Tensile strength and stiffness properties of additively manufactured PET-G polymer-based composite plates reinforced with different weight fractions of short carbon fibers

Circular economy innovation: A deep investigation on 3D printing of industrial waste polypropylene and carbon fibre composites

Transforming waste polypropylene (PP) and waste carbon fibre into upcycled composite materials for additive manufacturing represents an ideal circular economy challenge. An optimized method for material extrusion and 3D printing was developed to overcome adhesion and warpage challenges during printing. The study explored the impact of varying waste carbon fibre weight fractions (0 wt%, 2 wt%, 5 wt%, 8 wt%, 15 wt%, and 25 wt%), firstly on the properties of filament and then on printability and mechanical properties of printed specimens. Optimized extrusion parameters yielded the successful fabrication of fibre-reinforced filaments. Micro-level assessment of the polymer revealed a decrease in mechanical properties due to thermal processes during filament making and 3D printing. Microstructural analysis, along with optical and scanning electron microscopy, provided insights into inter-bead voids, debonding, fibre dispersion, fracture modes, and filament/sample quality. Differential Scanning Calorimetry indicated slight matrix degradation during filament extrusion, leading to slightly reduced melting and crystallization temperatures.

Role of fibre weight fraction on low-velocity impact characteristics of abaca fibre reinforced bio-composites

This work involved an experimental study on Abaca fibre bio-composites subjected to a low-velocity impact test at 2.42 m/s to study the effect of fibre weight fraction on the impact performance. The abaca fibre reinforced composite (AFRC) specimens were fabricated with a 10% increment of fibre, varying from Wf = 20% to 50%, and their impact properties compared with each other. The impact properties such as force-time history, energy-time history, Coefficient of Restitution (CoR), Energy Loss Percentage (ELP) and Energy Absorption Ratio (EAR) were studied. A significant change in impact force and energy absorption was found as the fibre content increased in the composite. The findings show a good relationship between fibre weight fractions, composite laminate stiffness, impact load and total absorbed energy. The experimental results of the impact test show that the composite specimen with Wf = 40% has high impact energy absorption capacity with 4. 09 J 92.94 N and 4.09 J, EAR of 39.94%, CoR of 0.77 and ELP of 40.04%. Low fibre weight fraction composite has shown brittle failure, and high fibre weight fraction has shown ductile behaviour. Scanning electron microscopy (SEM) based study was used for post-impact damage analysis.

Ultrasonic non-destructive inspection method for glass fibre reinforcement polymer (GFRP) hull plates considering design and construction characteristics

The design and construction characteristics, including glass fibre weight fraction ( Gc), number of single-ply layers, fabric combination, and fabrication quality, of glass fibre reinforcement polymer (GFRP) hull plates affect ultrasound propagation characteristics, such as ultrasonic velocity and attenuation, thereby influencing the accuracy of ultrasonic non-destructive test results. Therefore, this study is to propose a method to decrease the ultrasonic test errors of GFRP hull plate by using statistical method. The GFRP specimens with Gc of approximately 30–50 wt%, thicknesses of approximately 5–20 mm, and different fabric combinations were prepared using the hand lay-up method, considering the general design–construction characteristics. Further, an ultrasonic velocity decision method for ultrasonic inspection was proposed considering the GFRP hull design-construction characteristics, such as Gc and number of single-ply layers of hull plate by multiple linear regression method. The results show that the proposed method can reduce the thickness measurement error from approximately 20%–30% to 1%–2%, compared to an existing ultrasonic inspection method, only considering the Gc effect on ultrasonic velocity, which indicates that the proposed test method is suitable for practical applications.

Stacking Sequence and Weight Fraction Effect on Tensile and Flexural Properties of Woven Jute and Woven Carbon-Jute Reinforced Polyester Composites

Hybrid composites are a category of composites in which more than one types of fiber are used to reinforce the matrix. In this work, the mechanical properties of jute woven & and carbon-jute woven reinforced polymer matrix hybrid composites were evaluated to assess a comparative study between the two configurations varying the stacking sequences. Specimens of composites were prepared by hand layup process. To observe the effect of fiber weight fraction on properties, two types of composites were made having matrix-fiber weight fractions of 85:15 & and 80:20. Moreover, by altering the stacking sequences of the composites, these properties were also examined for the carbon-jute reinforced polymer matrix composites. It was observed that a hybrid jute-carbon composite having a stacking sequence of j/c/j/c/j and weight fraction ratio of 80:20 exhibited a better tensile strength of 108.795(10.885) MPa and Young’s modulus of 6.052(0.489) GPa. Superior flexural strength of 150.41 (±7.501) MPa and flexural modulus of 6.845(±0.825) GPA were found in hybrid jute-carbon composite having stacking sequence of j/c/j/c/j/c/j/c/j that has a weight fraction ratio of 80:20. In both cases, better mechanical properties were found for hybrid composites with higher fiber content and having alternate stacking sequences.

A powder-scale multiphysics framework for powder bed fusion of fiber-reinforced polymer composites

Additive manufacturing of fiber-reinforced polymer composites has garnered great interest due to its potential in fabricating functional products with lightweight characteristics and unique material properties. However, the major concern in polymer composites remains the presence of pore defects, as a thorough understanding of pore formation is insufficient. In this study, a powder-scale multiphysics framework has been developed to simulate the printing process of fiber-reinforced polymer composites in powder bed fusion additive manufacturing. This numerical framework involves various multiphysics phenomena such as particle flow dynamics of fiber-reinforced polymer composite powder, infrared laser–particle interaction, heat transfer, and multiphase fluid flow dynamics. The melt depths of one-layer glass fiber–reinforced polyamide 12 composite parts fabricated by selective laser sintering are measured to validate modelling predictions. The numerical framework is employed to conduct an in-depth investigation of pore formation mechanisms within printed composites. Our simulation results suggest that an increasing fiber weight fraction would lead to a lower densification rate, larger porosity, and lower pore sphericity in the composites.

Electrically Equivalent Head Tissue Materials for Electroencephalogram Study on Head Surrogates

With the recent advent of smart wearable sensors for monitoring brain activities in real-time, the scopes for using Electroencephalograms (EEGs) and Magnetoencephalography (MEG) in mobile and dynamic environments have become more relevant. However, their application in dynamic and open environments, typical of mobile wearable use, poses challenges. Presently, there is limited clinical data on using EEG/MEG as wearables. To advance these technologies at a time when large-scale clinical trials are not feasible, many researchers have turned to realistic phantom heads to further explore EEG and MEG capabilities. However, to achieve translational results, such phantom heads should have matching geometric features and electrical properties. Here, we have designed and fabricated multilayer chopped carbon fiber–PDMS reinforced composites to represent phantom head tissues. Two types of phantom layers are fabricated, namely seven-layer and four-layer systems with a goal to achieve matching electrical conductivities in each layer. Desired electrical conductivities are obtained by varying the weight fraction of the carbon fibers in PDMS. Then, the prototype system was calibrated and tested with a 32-electrode EEG cap. The test results demonstrated that the phantom effectively generates a variety of scalp potential patterns, achieved through a finite number of internal dipole generators within the phantom sample. This innovative design holds potential as a valuable test platform for assessing wearable EEG technology as well as developing an EEG analysis process.

The Effect of Thermal Residual Stress on the Stress State in a Short-Fiber Reinforced Thermoplastic

Upon their cooling and solidification, significant thermal residual stresses can develop in short-fiber reinforced thermoplastics due to the mismatch in coefficient of thermal expansion between fiber and matrix. In this study we set out to investigate this effect numerically. The build-up of thermal residual stresses is modeled by expanding a well-established constitutive model, the Eindhoven glassy polymer (EGP) model, with thermal expansion. The experimentally measured thermal residual stresses can be described using an effective glass-transition temperature and a constant coefficient of thermal expansion without the need for complex equilibrium kinetics associated with the glass transition itself. Subsequently, the influence of thermal residual stress on the deformation behavior for a short-fiber reinforced thermoplastic is studied employing multi-fiber representative volume elements (RVEs) for different fiber-weight fractions. The micromechanical models are evaluated on the importance of thermal residual stresses on the local and nominal stress state. From these analyses it can be concluded that the thermal residual stresses should be accounted for when assessing the quantitative local stress state and are therefore essential when local mechanisms are studied. In contrast, thermal residual stresses are not required to capture the nominal transient stress–strain response.

Investigation of viscoelastic behavior of Abaca-reinforced epoxy composites

Natural fiber-based composites demonstrate excellent and comparable static and dynamic mechanical properties to conventional materials, such as steel and aluminum. They also extend their applications to aeronautical, sports equipment, and marine fields. This experimental study aims to find the effect of untreated and treated Abaca-reinforced epoxy composites on the viscoelastic behavior and the optimum combinations of fiber and resin to produce better bonding efficiency. The different specimens used for this study were pure epoxy, untreated, and chemically treated composite specimens. The four weight percentages of Abaca fibers are 10%, 20%, 30%, and 40% used to prepare composite specimens. Similarly, four different sodium hydroxide (NaOH) concentrations, 4, 6, 8, and 10 wt. %/vol. %, have been used for the chemical treatment of fibers. The storage modulus of Abaca-reinforced epoxy composite specimen has been investigated with respect to temperature and fiber content. The result shows that the 30% weight fraction of fibers with chemically (8 wt. %/vol. %) treated fiber-reinforced epoxy specimen produces 41.67% higher storage modulus than the 10% weight fraction of fibers content of composite specimens. Fourier-Transform Infrared Spectroscopy (FTIR) broad transmittance has been used to distinguish the raw and chemically treated fibers. FTIR results reveal the removal of functional groups after NaOH treatment.

Natural Fiber Reinforced Shoe Midsoles with Balanced Stiffness/Damping Behavior.

The comfort of walking depends heavily on the shoes used. Consequently, the midsole of shoes is designed in such a way that it can dampen force peaks during walking. This significantly increases the overall wellness during walking. Therefore, the midsole usually consists of rubber-like polymers, such as polyurethane and ethylene-vinyl acetate copolymer. Furthermore, the manufacturing process of these polymers results in a foam-like structure. This further enhances the damping behavior of the material. Nevertheless, it would be desirable to find a cheap and sustainable method to enhance the damping behavior of the shoe midsole. The purpose of this work is to see if hemp fibers, which are part of the polymer matrix material, could improve the stiffness without losing the damping behavior. The mechanical properties of such prepared fiber-reinforced composites were characterized by quasi-static tensile testing and dynamic mechanical analysis. The mechanical properties were examined in relation to the fiber type, weight fraction, and type of polyurethane used. Furthermore, the investigation of the embedding of these fibers in the polymer matrix was conducted through the utilization of optical and electron microscopy.

Flax fibre reinforced alginate poloxamer hydrogel: assessment of mechanical and 4D printing potential.

The mechanical and printing performance of a new biomaterial, flax fibre-reinforced alginate-poloxamer based hydrogel, for load-bearing and 4D printing biomedical applications is described in this study. The-self suspendable ability of the material was evaluated by optimising the printing parameters and conducting a collapse test. 1% of the flax fibre weight fraction was sufficient to obtain an optimum hydrogel composite from a mechanical perspective. The collapse test showed that the addition of flax fibres allowed a consistent print without support over longer distances (8 and 10 mm) than the unreinforced hydrogel. The addition of 1% of flax fibres increased the viscosity by 39% and 129% at strain rates of 1 rad s-1 and 5 rad s-1, respectively, compared to the unreinforced hydrogel. The distributions of fibre size and orientation inside the material were also evaluated to identify the internal morphology of the material. The difference of coefficients of moisture expansion between the printing direction (1.29 × 10-1) and the transverse direction (6.03 × 10-1) showed potential for hygromorphic actuation in 4D printing. The actuation authority was demonstrated by printing a [0°; 90°] stacking sequence and rosette-like structures, which were then actuated using humidity gradients. Adding fibres to the hydrogel improved the repeatability of the actuation, while lowering the actuation authority from 0.11 mm-1 to 0.08 mm-1. Overall, this study highlighted the structural and actuation-related benefits of adding flax fibres to hydrogels.