Abstract Aluminium based metal matrix composites with several reinforcement (Hybrid MMC’s) have countless advantages of satisfying current requirement of engineering applications due to their enhanced mechanical properties like tensile strength, hardness, toughness etc. The functioning of these type of material depend on the choice of right combination of filler particle. This research work deals with examination on mechanical behaviour of aluminium alloy (AA6061) composites fabricated with hematite and titanium dioxide particles. Semi-automatic stir casting technique was employed for fabrication of aluminium based hybrid composites by changing hematite in 2, 3, 4% by weight and titanium dioxide 1, 3, 5% by weight. A nine composites sample plates were fabricated. As per standard dimensions of ASTM, the sample specimen was cleaned by polishing over emery paper. Physical properties (density and void content), mechanical properties such as impact strength, tensile strength, hardness and sliding wear behaviour (Pin on disc tribometer) characterisation were carried out and examined. The Taguchi experiment design was used to develop experimental runs have input parameter sliding distance (1000, 1500, 2000 m), normal load (10, 15, 20 N) and reinforcement contents (2–4% by wt. Fe2O3 and 1–5% by wt. % TiO2). The worn surface structure studies were carried out to know the mechanism of the wear using Field Emission Scanning Electron Microscope (FESEM) along with Energy-dispersive X-ray spectroscopy (EDS) which indicate elemental composition and dispersion on the material surface.