The operating slip systems and flow behavior of single crystalline Al 66.8Ti 27.4Fe 5.8, a two phase Ll 2 + Al 2Ti material, was investigated as a function of temperatures using specimens with compressive axes near [001], [ 1 13], [ 1 12], [013] and [ 1 33]. The material shows a very limited compressive ductility, and fracture occurs by cleavage along planes of low indices, such as {011}, {001}, {013} and {111}. Slip occurs exclusively on the octahedral slip systems at low temperatures, and on both octahedral and cube systems at high temperatures. A transition in operating slip systems from octahedral slip to cube slip, similar to the one seen in Ni 3Al-type alloys, occurs as the temperature increases and as the orientation of the specimens change from near-[001] to near-[ 1 11]. The transition in slip system is attributed to the hardening effect of the Al 2Ti precipitates, rather than to the anisotropy of APB energy on cube and octahedral slip planes of the matrix. Because of the large hardening effect of the Al 2Ti, the two phase material is substantially stronger than single Ll 2 phase materials. The shape (but not the level) of the flow stress-temperature curve for the two phase material resembles that of the single phase Ll 2 material at low and intermediate temperatures. At high temperatures, however, the flow stress of the two phase material exhibits a sharp decrease, a feature which is not observed in the single phase Ll 2 materials and can be correlated with a continuous dissolution of the Al 2Ti precipitates at high temperatures.
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