It has been widely reported that the application of high-level ultrasonic energy during dispersion process of carbon nanotube causes damage on the carbon nanotube and reduces its mechanical performance. However, if the amount of ultrasonic energy is insufficient, the quality of carbon nanotube dispersion becomes poorer so that the effect caused by carbon nanotube reinforcement is minimized. In this work, the step sonication process, which divides a prolonged sonication into a few separate cycles while maintaining the same level of ultrasonic energy, is applied since this process can improve dispersion of carbon nanotube without causing serious damage. Commercially available polycarboxylate ester, polycarboxylate, and air entraining agent were used as dispersing agents. The effect caused by step sonication and type of dispersing agent on dispersion quality of multi-walled carbon nanotube was evaluated, and their impacts on mechanical strength development of cement paste were analyzed. According to the experimental results, step sonication process improved the quality of multi-walled carbon nanotube dispersion when polycarboxylate ester and polycarboxylate were used. Step sonication process was found to be more effective for multi-walled carbon nanotube suspension with higher concentration. Among all dispersing agents, air entraining agent was found to be the best dispersing agent showing 2 times higher UV absorption peak than polycarboxylate and polycarboxylate ester, but the application of air entraining agent caused 40–65% reduction in compressive strength due to the air entrainment. It was also found that dispersion quality of multi-walled carbon nanotube affected flexural strength more significantly than compressive strength.
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