Abstract
Zinc oxalate, [Zn(C 2O 4)·2H 2O] was used as a precursor to prepare zinc oxide nanotriangles by thermal decomposition. The different combinations of triphenylphosphine, and oleylamine were added as surfactants to control the particle size. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), photoluminescence spectroscopy (PL), Fourier transform infrared (FT-IR) spectroscopy, Ultraviolet–visible (UV–vis) spectroscopy and X-ray photoelectron spectroscopy (XPS). The synthesized ZnO nanoparticles have a hexagonal zincite structure.
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