Abstract

The title compound, C27H37NO7, is a Daphniphyllum alkaloid isolated from a branch of Daphniphyllum macropodum Miq. All of the five-membered rings adopt envelope conformations while the six- and seven-membered ring adopt chair conformations. Classical inter­molecular O—H⋯O and weak C—H⋯N hydrogen bonds are present in the crystal structure.

Highlights

  • The title compound, C27H37NO7, is a Daphniphyllum alkaloid isolated from a branch of Daphniphyllum macropodum Miq

  • For the chemical structure of the title compound established from NMR and MS data, see: Li et al (2009)

  • R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger

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Summary

Oxford Xcalibur diffractometer with an Eos CCD detector

The title compound, C27H37NO7, is a Daphniphyllum alkaloid isolated from a branch of Daphniphyllum macropodum Miq. All of the five-membered rings adopt envelope conformations while the six- and seven-membered ring adopt chair conformations. C—H N hydrogen bonds are present in the crystal structure

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This project was supported by grants from the PhD
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