Abstract
Reaction of carbon monoxide with [Rh{C(N 2)SiMe 3}(PEt 3) 3] gives [Rh{C(CO)SiMe 3}(CO)(PEt 3) 2] ( 3) in a high yield, Wolff-like rearrangement process. This is the first Rh I η 1'-ketenyl complex which has been characterized by 1H, 13C, 31P NMR and IR spectroscopies.
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