Abstract
A simplified and efficient assembly for the preparative photochemistry is described. The apparatus was tested in some classical organic photochemical reactions such as photobleaching of riboflavin, and photo reduction of the benzophenone, as well as in some organometallic reactions: photodimerization of pentacarbonyliron and in inorganic reactions: photo reduction of silver and platinum salts or complexes. Two new protocols were described: the photo reduction of copper (II) chloride and the first photochemical synthesis of ferricenium tetrachloroferrate. We demonstrated that the assembly may be useful in organic, inorganic and organometallic preparative photochemistry.
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