Abstract
Thermal decompositions of NaClO4 and KClO4 were followed by simultaneous TS-DTA and thermomicroscopy. For NaClO4 TS curves corresponding to melting/decomposition and solidification of molten NaCl were found to consist of six peaks. During decomposition of KClO4, three TS peaks appeared. The origin of these TS peaks is discussed on the basis of thermomicroscopic observations during which melting of the particles, evolution of bubbles of different sizes, formation of solid products of varied morphologies, vigorous vibration of these solids, and precipitation of NaCl or KCl were observed.
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