Abstract
N-(t-butoxycarbonyl)-3-methylbenz[f]indole,1, C18H19NO2, crystallizes in orthorhombic space groupPna21 witha=6.0338(2),b=24.839(4),c=10.2481(7) A,V=1535.9(3) A3,Z=4. The structure was refined toR=0.051 for 2007 observed reflections. The benz[f]indole ring system is nearly planar, exhibiting mean deviation of 0.048 A. The ester plane of thet-butoxycarbonyl substituent is nearly coplanar with the benz[f]indole ring system, forming a C−N−C=O torsion angle with magnitude 10.6(5)0.N-benzenesulfonyl-4-bromo-3-methyl-benz[f]indole,2, C19H14BrNO2S crystallizes in triclinic space groupP−1 witha=8.1400(5),b=10.0587(8),c=10.8863(7) A, α=89.927(7), β=110.495(5), γ=96.846(6)0,V=828.2(3) A3,Z=2. The structure was refined toR=0.050 for 2653 observed reflections. The benz[f]indole ring system is nearly planar, with mean deviation 0.016 A, and forms a dihedral angle of 80.93(9)0 with the phenyl plane.
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