Abstract
An interfacial route is described to form composites of molybdenum disulfide with metals. Metal deposition occurs at the liquid| liquid interface, on to the pre-adsorbed MoS2 film. The method is exemplified via the interfacial deposition of Cu and Pd at the MoS2-modified water/1,2,-dichlorobenzene interface, under electrochemical control (interface between two immiscible electrolyte solutions). Differences in morphology between the two metals are related to their differing modes of growth. The voltammetric measurements were analysed to elucidate the effect of the interfacial MoS2 film on the reduction and growth of the metals. Overall, the MoS2 film was found to impact the metallic deposition reaction, and the effect depends on the nature of the metallic precursor.
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