Abstract
The vanadium(V) peroxo phosphato complex K 7[V 4O 4(O 2) 8(PO 4)]·9H 2O has been obtained from the KVO 3KH 2PO 4KOHH 2O 2H 2OC 2H 5OH system. The X-ray structural analysis revealed a tetranuclear anionic structure in which two dinuclear [V 2O 2(O) 2) 2( μ- η 1 : η 2-O 2) 2] units are connected by the μ 4-PO 4 group.
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