Abstract
A method is presented for the determination of molybdenum by extraction of its thiocyanate complex with methyl isobutyl ketone. The method is accurate to ±4% or 3 μg of molybdenum, whichever is greater. The only elements which cause interference are rhenium (serious), platinum, palladium, rhodium, selenium and tellurium. The method has been applied to a number of standard samples with excellent results.
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