Abstract
A method is described for the determination of molybdenum by extraction of its thiocyanate complex with methyl isobutyl ketone. The method is accurate to ±4% or ±3 micrograms of molybdenum, whichever is greater. The accuracy and sensitivity can be improved by appropriate choice of sample size, volume of extract and/or cell length. Of 68 elements investigated, only rhenium, platinum, palladium, rhodium, vanadium, and tellurium interfere in 10-mg amounts. Of these, only rhenium interferes seriously.
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