Abstract
The reaction of nickel(II) thiocyanate with an excess of pyridazine leads to single crystals of the title compound, [Ni(NCS)2(C4H4N2)4]·2C4H4N2. The NiII cations are coordinated by two terminal N-bonded thiocyanate anions (trans) and four pyridazine ligands in a slightly distorted octahedral geometry. The discrete complexes are arranged into layers parallel to the ab plane which are separated by additional non-coordinated pyridazine ligands.
Highlights
The reaction of nickel(II) thiocyanate with an excess of pyridazine leads to single crystals of the title compound
The discrete complexes are arranged into layers parallel to the ab plane which are separated by additional noncoordinated pyridazine ligands
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2)
Summary
R factor = 0.032; wR factor = 0.084; data-to-parameter ratio = 16.5. The reaction of nickel(II) thiocyanate with an excess of pyridazine leads to single crystals of the title compound,. The NiII cations are coordinated by two terminal N-bonded thiocyanate anions (trans) and four pyridazine ligands in a slightly distorted octahedral geometry. The discrete complexes are arranged into layers parallel to the ab plane which are separated by additional noncoordinated pyridazine ligands
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